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| Herbert C.G., Johnstone R.A.W. — Mass Spectrometry Basics |
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| Предметный указатель |
Mass measurement, resolution of mass spectrometers 271—272
Mass measurement, value of accurate mass measurement 271
Mass spectrometer(s) see also “Computers and transputers in mass spectrometers”
Mass spectrometer(s), as source of data 317
Mass spectrometer(s), AutoSpec-TOF® 154 156 157
Mass spectrometer(s), calibration 296
Mass spectrometer(s), condensation of atmospheric moisture onto 278
Mass spectrometer(s), contamination of 18
Mass spectrometer(s), double-focusing 195
Mass spectrometer(s), factors important in choosing between quadrupole and magnetic-sector 186
Mass spectrometer(s), hybrid 243
Mass spectrometer(s), identification of structure of sample analyzed by 15
Mass spectrometer(s), ion cyclotron resonance 282
Mass spectrometer(s), isotope ratio 349
Mass spectrometer(s), magnetic/electric-sector see “Ion optics of magnetic/electric-sector mass spectrometers”
Mass spectrometer(s), objectives in buying 275
Mass spectrometer(s), operation of under high vacuum 372
Mass spectrometer(s), quadrupole 205 255 264
Mass spectrometer(s), resolution of 271
Mass spectrometer(s), schematic diagram of 254 262
Mass spectrometer(s), solution flowing into front end of 55
Mass spectrometer(s), TOF 191
Mass spectrometer(s), TOF, collection of ions using 213
Mass spectrometer(s), TOF, major advantage of 192
Mass spectrometer(s), TOF, traces of material introduced into 209
Mass spectrometer(s), TOF, under everyday conditions 281
Mass spectrometer, choice of 275—285
Mass spectrometer, complexity of sample 276—277
Mass spectrometer, ionization methods 282—285
Mass spectrometer, mass analyzers 280—282
Mass spectrometer, objectives in buying mass spectrometer 275—276
Mass spectrometer, overall view of choices 285
Mass spectrometer, sample volatility, polarity, and thermal stability 278—280
Mass spectrometer, types of sample 276
Mass spectrometry (MS) 4 71 77 245
Mass spectrometry (MS), books on 449—452
Mass spectrometry (MS), connection between LC and 262
Mass spectrometry (MS), electron ionization 13
Mass spectrometry (MS), history of 275
Mass spectrometry (MS), isotope ratios in routine 343
Mass spectrometry (MS), magnetic-sector see “Magnetic-sector mass spectrometry linked
Mass spectrometry (MS), publications containing occasional papers related to 455
Mass spectrometry (MS), quadrupole see “Quadrupole mass spectrometry linked
Mass spectrometry (MS), regular publications in 453
Mass spectrometry (MS), secondary ion 17 260
Mass spectrometry (MS), structure of atomic building blocks for 336
Mass spectrometry (MS), tandem 226 see
Mass spectrometry definitions and terms 429—447
Mass spectrometry definitions and terms, analyzers 429—130
Mass spectrometry definitions and terms, common abbreviations 444—447
Mass spectrometry definitions and terms, data system 430—431
Mass spectrometry definitions and terms, ion detection and sensitivity 436—437
Mass spectrometry definitions and terms, ion/molecule reactions 443—444
Mass spectrometry definitions and terms, ionization nomenclature 437—439
Mass spectrometry definitions and terms, sample introduction 432—433
Mass spectrometry definitions and terms, scanning of spectra 433—436
Mass spectrometry definitions and terms, types of ions, ion structures 440—443
Mass spectrometry/mass spectrometry (MS/MS) 288
Mass spectrometry/mass spectrometry (MS/MS), applications, quadrupole and magnetic sectors in 186
Mass spectrometry/mass spectrometry (MS/MS), experiment, diagrammatic representation of 198
Mass spectrometry/mass spectrometry (MS/MS), hybrid instrumentation necessary for 282
Mass spectrometry/mass spectrometry (MS/MS), methods, examination of mixture by 59
Mass spectrometry/mass spectrometry (MS/MS), studies, hybrid mode of operation for 160
Mass spectrum, attribute of 237
Mass spectrum, carbon compound 16
Mass spectrum, distorted 255
Mass spectrum, effect of isotope pattern on 340
Mass spectrum, FAB 21 22
Mass spectrum, hemoglobin 58
Mass spectrum, high-resolution 273
Mass spectrum, LSIMS 22
Mass spectrum, patterns of isotopes in 16
Mass, analyzer, transfer of ions to 95
Mass, chromatogram 258 266
Mass, filters 211 231
Mass, organometallics, vaporization of 58
Mass, resolution, unrealistic consideration of 281
Mass, separation 231
Mass, spectra, closeness of fit of 300
Mass, spectra, data, manipulation of 322
Mass, spectra, recording of 255 264
Mass-to-charge (m/z) ratio 13 14 72 219 291
Matrix material 9
Matrix-assisted laser desorption ionizatio (MALDI) 9 119 153
Matrix-assisted laser desorption ionizatio (MALDI), experiment 10
Matrix-assisted laser desorption ionizatio (MALDI), ionization/inlet systems 161
Matrix-assisted laser desorption ionizatio (MALDI), mass analyzers used with 284
Matrix-assisted laser desorption ionizatio (MALDI), sample preparation for 12
Matrix-assisted laser desorption ionizatio (MALDI), secondary ionization with 11 12
Matrix-assisted laser desorption ionizatio (MALDI), vaporization of materials through use of 280
MCN see “Microconcentric nebulizers”
McReynolds number 248
Measurement, precision and accuracy of 361
Measurement, units of 361
Messenger ribonucleic acid (mRNA) 327
Metastable ions, abundances of metastable ions 227
Metastable ions, disadvantages of low abundance of metastable ions 228
Metastable ions, enhanced fragmentation 228
Metastable ions, field free zones and formation of metastable ions 226—227
Metastable ions, origin and uses of 225—229
Metstable ion(s), 180 see also “Quadrupole mass spectrometry linked
Metstable ion(s), abundances of 227 229
Metstable ion(s), decomposition 226 239 244
Metstable ion(s), formation of 226
Metstable ion(s), how quadrupoles can be used to examine 233
Metstable ion(s), linked scanning of 235
Micro-ultrasonic nebulizers 148
MicroChannel array, diagram illustrating element of 221
MicroChannel elements, ion mass range 215
MicroChannel multipoint ion collector 160
MicroChannel plate collectors 197 198 216 221
Microconcentric nebulizers (MCN) 142
Microprocessor 313
Mirror, nonreflective 127
Mode locking 126 128
Molecule(s), agglomerations 108
Molecule(s), collision between sample 62
Molecule(s), dye 132
Molecule(s), fluorescent 133
Molecule(s), interaction 130
Molecule(s), ionization of solute 79
Molecule(s), mass, calculation of 270
Molecule(s), protonated solvent 62
Molecule(s), relative molecular mass of 270
Molecule(s), retention time for in chromatography 248
Molecule(s), substrate 386
Molecule(s), triplet-state 131
Momentum transfer 18
Monochromatic radiation 122
Monochromators 119
mRNA see “Messenger ribonucleic acid”
ms see “Mass spectrometry”
MS/MS see “Mass spectrometry/mass spectrometry”
Multibase arithmetic 303
Multichannel plate array 220
Multiphoton waveform, amplitude of 120
Multiple ion recording 260
Multipoint collectors of ions, array elements 215
Multipoint collectors of ions, arrays and microchannel plates 213—214
Multipoint collectors of ions, comparison of 211—217
Multipoint collectors of ions, elements of array and microchannel plates 214—215
Multipoint collectors of ions, mirochannel elements 215—216
Multipoint collectors of ions, uses of array and microchannel collectors 216
Muscular dystrophy, use of DNA sequence data to investigate 329
Nanotube sprays 66
National Institute for Standards and Technology (NIST) 354
National Institutes of Health (NIH) 301
National Pollution Discharge Elimination System 296
Naturally occurring isotopes 339 341 344—345
Nebulization, concept 106
| Nebulization, inlets 108
Nebulizer(s) 77 137—152
Nebulizer(s), Babington 145
Nebulizer(s), background 137
Nebulizer(s), concentric tubular 142—144
Nebulizer(s), cross-flow 141 144—147
Nebulizer(s), designs of 139
Nebulizer(s), electrospray nebulization 150—151
Nebulizer(s), frit 146
Nebulizer(s), general principles of aerosol formation 138—139
Nebulizer(s), high-efficiency 143
Nebulizer(s), introduction of sample solution via 152
Nebulizer(s), micro-ultrasonic 148
Nebulizer(s), microconcentric 142
Nebulizer(s), nature of aerosol 137—138
Nebulizer(s), oscillating-capillary 149
Nebulizer(s), parallel-path 146
Nebulizer(s), piezoelectric transducer 148
Nebulizer(s), pneumatic 139—141 148
Nebulizer(s), spray and desolvation chambers 152
Nebulizer(s), systems, adjuncts to 152
Nebulizer(s), thermospray 106 149—150
Nebulizer(s), types 106
Nebulizer(s), ultrasonic 147—149
Needle tip electrode, design of 24
Neodymium lasers 134
Neon, excited state of 131
Neutral species 48 237
Neutron, characteristics of 338
Nicotinic acid 9
Nier — Johnson geometry 238
NIH see “National Institutes of Health”
NIH-EPA mass spectral library 301
NIST see “National Institute for Standards and Technology”
NIST library 257 266
Nonradioactive isotopes 354
Nozzle, common types of 143
Nuclear bombs, manufacture of 369
Nuclear power reactors 353
Nuclear waste, discharges of 369
Nucleosides, examination of 26
Nucleosides, GC and 251
Nucleosides, vaporization of 58
Occam 309 314 315
Octopole configuration 382
Oligonucleotides 279
Oligopeptide 331
Organometallics, GC and 251
Organometallics, isotope patterns for 350
Orthogonal time-of-fiight instruments, hybrid 153—156
Osmium tetroxide, volatility of 100
Outliers 361
Oxidation, prevention of 113
Oxygen, irradiation of 130
Parallel processing, of information 311 313
Parallel-path nebulizer 146
Particle-beam interface 77—80 393
Particle-beam interface, background 77
Particle-beam interface, efficiency 79
Particle-beam interface, evacuation chamber 77
Particle-beam interface, first skimmer 78
Particle-beam interface, ion source 79
Particle-beam interface, ionization 79
Particle-beam interface, nebulizer 77
Particle-beam interface, second skimmer 78—79
Particle-beam interface, similarity to other interfaces 79—80
Pascal 309 314
Passive Q-switching 127 128
PC see “Personal computer”
PeeDee belemnite (PDB) 354
Peptide(s), creation of overlap 331 333
Peptide(s), Edman sequential degradation of 332
Peptide(s), examination of 26 294
Peptide(s), FD and 27
Peptide(s), formation of 330
Peptide(s), GC and 251
Peptide(s), identification of amino-terminal residue of 332
Peptide(s), interpretation of mass spectrum of 333
Peptide(s), mixtures, analysis of 293
Peptide(s), vaporization of 58
Peptides and proteins, analysis of by mass spectrometry 287—294
Peptides and proteins, dynamic FAB 288
Peptides and proteins, fast-atom bombardment 287—288
Peptides and proteins, mass spectrometry/mass spectrometry 288—290
Peptides and proteins, other ion sources 290—294
Perfluorinated hydrocarbons 272
Personal computer (PC) 308
Phenylthiohydantoin (PTH) 331
Photodiodes 117
photoelectric effect 36 40
Photoflash 121
Photon(s), fluorescent 132
Photon(s), interaction of excited-state atom with 126
Photon(s), light sources emitting 119
Photon(s), waves 120
Piezoelectric devices 107
Piezoelectric spark 40
Piezoelectric transducer nebulizers 148
Planck's constant 117
Plasma torch (FT), cold plasma conditions and plasma cage 94—95
Plasma torch (FT), construction of plasma torch 88—89
Plasma torch (FT), interface 95
Plasma torch (FT), plasma flame 89—90
Plasma torch (FT), processes occurring in plasma after introduction of sample 92—94
Plasma torch (PT) 10 87—96 284
Plasma torch (PT), introduction of solids 110—116
Plasma torch (PT), introduction of solids, direct sample insertion 114—116
Plasma torch (PT), introduction of solids, electrical discharge ablation 113—114
Plasma torch (PT), introduction of solids, electrical heating 114
Plasma torch (PT), introduction of solids, laser devices 111—112
Plasma torch (PT), problems of sample introduction 109—110
Plasma torch (PT), sample inlets for, solid inlets 109—116
Plasma torches, desolvation chambers 107—108
Plasma torches, direct insertion methods 105
Plasma torches, electrothermal heating methods 106
Plasma torches, introduction of gases 98—102
Plasma torches, liquid inlets 104
Plasma torches, nebulizer methods 106—107
Plasma torches, problems of sample introduction 97—98 103—104
Plasma torches, sample inlets for, gases 97—102
Plasma torches, sample inlets for, liquid inlets 103—108
Plasma, cage 94
Plasma, flame 89 90
Plasma, flame, diameter of 98 104 110
Plasma, flame, direct insertion of sample into 105
Plasma, flame, introduction of samples into 97 103 109
Plasma, flame, method of direct insertion of sample into 115
Plasma, temperature of 91
Plasmaspray (PS) 73 79
Plasmaspray (PS), interfaces see “Thermospray and plasmaspray interfaces”
Plasmaspray (PS), ionization 61
Plasmaspray (PS), ions passing into mass spectrometer analyzer from 74
Plasmaspray (PS), LC/MS with 75
Plutonium contamination 369
PN see “Pneumatic nebulizers”
Pneumatic nebulizers (PN) 139 141 148
Pockels cell 127
Point detection 201
Point ion collectors 201—204 206
Poiseuille's formula 141
Polar carboxylic acids 283
Polar substances, vaporization of 58—59
Polycyclic aromatic hydrocarbons 5
Polymers, FD and 27
Polypeptide 331
Population inversion 124
Potassium/argon dating 368
PP1NICI 3
Precursor ions 198 233 241
Product ion scans 233
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