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Herbert C.G., Johnstone R.A.W. — Mass Spectrometry Basics
Herbert C.G., Johnstone R.A.W. — Mass Spectrometry Basics



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Название: Mass Spectrometry Basics

Авторы: Herbert C.G., Johnstone R.A.W.

Аннотация:

Mass Spectrometry Basics is a pedagogy for novice practitioners and those with little or no experience in the field of mass spectrometry. It includes information on ionisation processes, techniques, instruments, and general MS and combined MS applications. The text also has an extensive reference section and quick guides that highlight the essential information discussed in each chapter.


Язык: en

Рубрика: Физика/

Статус предметного указателя: Готов указатель с номерами страниц

ed2k: ed2k stats

Год издания: 2002

Количество страниц: 474

Добавлена в каталог: 03.10.2006

Операции: Положить на полку | Скопировать ссылку для форума | Скопировать ID
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Предметный указатель
EI      see “Electron ionization”
Electric charges      337
Electric discharge, ablation      113
Electric discharge, effect      131
Electric fields, stray      372
Electric potential      387
Electric signal, digitized      306
Electrical heating      114
Electrode(s), inhomogeneous RF field applied to      380
Electrode(s), shapes, effect of on discharge      38
Electron ionization (EI)      1 13—16 61 71 225 275
Electron ionization (EI), /CE switching process      4 5
Electron ionization (EI), ion source      14—15
Electron ionization (EI), ionization process      13
Electron ionization (EI), isotopes      16
Electron ionization (EI), mass spectrum      14
Electron ionization (EI), mass-to-charge ratio      13—14
Electron ionization (EI), spread in kinetic energy in      177
Electron ionization (EI), suitability of beam entering ion chamber for      79
Electron ionization (EI), yield of molecular ions during      283
Electron multiplier(s), assemblage of single-point      213
Electron multiplier(s), idealized face view of set of      213
Electron multiplier(s), ions directed onto first plate of      202
Electron(s)      337
Electron(s), acceleration of      36
Electron(s), actual drift velocities of      35
Electron(s), collisions between neutral sample molecules and      38
Electron(s), drift of      41
Electron(s), energy(ies), barrier against      23
Electron(s), energy(ies), idealized distribution of      41
Electron(s), fast-moving      93
Electron(s), major property of      337
Electron(s), transfer, ionization by      19
Electronic amplification      203
Electronic circuit, flip-flop      303 306
Electronic energy, of molecule      7
Electronic switching, binary code and      306
Electrophoresis      331
Electrospray (ES)      277 291
Electrospray (ES), /mass spectrometry (ES/MS)      138
Electrospray (ES), attribute of      284
Electrospray (ES), development of      291
Electrospray (ES), inlet/ion source, schematic diagram of      56
Electrospray (ES), ions formed in      167
Electrospray (ES), light of sight for conventional      67
Electrospray (ES), nebulizer (EN)      150
Electrospray (ES), spectrum, sickle-cell carrier cord blood globins      293
Electrospray (ES), transmission guides used in      377
Electrospray (ES), uses of      58
Electrospray ionization (ESI)      55—60
Electrospray ionization (ESI), convenience of      59
Electrospray ionization (ESI), differential solvent removal      56—57
Electrospray ionization (ESI), general comments      59—60
Electrospray ionization (ESI), multicharged ions      57—58
Electrospray ionization (ESI), uses of electrospray      58—59
Electrostatic analyzer (ESA)      177
Electrothermal vaporization (ETV)      106 114
Element(s), analysis, rare earth      351
Element(s), atomic masses for common      270
Element(s), atomic weights of      346—347
Element(s), number of isotopes occurring naturally for      349
Element(s), slower-evaporating      116
Element(s), volatile      116
Elution solvent      85
Emission, difference between normal emission and stimulated      123
EN      see “Electrospray nebulizer”
Energy(ies), collisional      29 376
Energy(ies), conversion of into light      121
Energy(ies), electronic      7
Energy(ies), filter      181
Energy(ies), ionization      47 49
Energy(ies), kinetic, ions having wrong      225
Energy(ies), kinetic, mass-selected main ion beam      198
Energy(ies), kinetic, product ion having insufficient      238
Energy(ies), kinetic, spread of in EI      177
Energy(ies), loss      123
Energy(ies), pulse of laser light of specific wavelength of      8
Energy(ies), rotational      7 94
Energy(ies), thermal      93
Energy(ies), transfer, inefficient      32
Energy(ies), translational      232
Energy(ies), vibrational      7
Environmental Protection Agency (EPA)      295
Environmental Protection Agency protocols      295—301
Environmental Protection Agency protocols, Contract Laboratory Program      296
Environmental Protection Agency protocols, environmental laws      295
Environmental Protection Agency protocols, protocols      296
Environmental Protection Agency protocols, sample analysis by GC/MS      296—301
Environmental science      351
Enzyme(s), heating of      331
Enzyme(s), restriction      328
Enzyme(s), uses of      333
EPA      see “Environmental Protection Agency”
EPA Contract Laboratory Program (CLP)      295 296
Equations of motion      183 186
Equilibrium process, thermodynamic concentration governing      49
ES      see “Electrospray”
ES/MS      see “Electrospray/mass spectrometry”
ESA      see “Electrostatic analyzer”
ESI      see “Electrospray ionization”
ETV      see “Electrothermal vaporization”
Evacuation chamber      77
evaporation      46
Evaporation, ion      51 ion
Evaporation, rate, variation in      116
Evaporation, sample      52
Evaporation, solvent      74 106
Event signals, storage of      222
Exact copying, gene      328
Exciplex      130
Excited state(s), atom, interaction of photon with      126
Excited state(s), levels      125
Excited state(s), methods of pumping to obtain      129
Excited state(s), populations of      124
Extraction cone      69
Faraday cup      202 204
Faraday dark space      34
fast switching      6
Fast-atom bombardment (FAB)      17 81 228 279 287
Fast-atom bombardment (FAB), /LSIMS ionization      82
Fast-atom bombardment (FAB), commonly used solvents for      21 83
Fast-atom bombardment (FAB), dynamic      86 163 263 288
Fast-atom bombardment (FAB), mass spectrum      21 22
Fast-atom bombardment (FAB), sensitivity of      290
Fast-atom bombardment (FAB), spread of kinetic energy in      177
Fast-atom bombardment and liquid-phase secondary ion mass spectrometry ionization      17—22
Fast-atom bombardment and liquid-phase secondary ion mass spectrometry ionization, atom or ion beams      18
Fast-atom bombardment and liquid-phase secondary ion mass spectrometry ionization, ionization process      18—20
Fast-atom bombardment and liquid-phase secondary ion mass spectrometry ionization, mass spectrum      21—22
Fast-atom bombardment and liquid-phase secondary ion mass spectrometry ionization, properties of solvent      20—21
Fast-ion bombardment (FIB)      279
FD      see “Field desorption”
fi      see “Field ionization”
fib      see “Fast-ion bombardment”
Field ionization and field desorption      23—27
Field ionization and field desorption, design of needle tip electrode      24—25
Field ionization and field desorption, field ionization      23—24
Field ionization and field desorption, practical considerations of field ionization/field desorption      25—27
Field ionization and field desorption, types of compounds examined by FI/FD      27
Field, desorption (FD)      23 26 27
Field, free region, metastable ions decomposing in      238 239 240
Field, ionization (FI)      23 237
Field, strength      23
Filament(s), assembly      46
Filament(s), elements useful for construction of      45
Filament(s), lamp      121
Flame, heat capacity of      105
Flame, instability      396 397
Flame, ionization      246 253
Flame, self-sustaining      95 103
Flame, solvent vapor entering      107
Flame, temperature, fluctuations in      98 109
Flash lamps      126 134
Fleming's left-hand rule      175 176
Flight tube      171
Flip-flop electronic circuit      303 306
Fluorocarbon      272
Fluorodecane, carbon atoms of      345
Fluorodecane, mass spectrum of molecular ion region of      344
Forbidden transition      125
FORTRAN      309 314
Fourier-transform ion cyclotron resonance (FTICR)      189 201 281
Fourier-transform techniques      274
Fractionation factors, variations in      358
Fragment ions      2 237 269
Fragmentation      3 105
Fragmentation, enhanced      228
Fragmentation, pathways      225
Fragmentation, random      20
Fragmentation, reactions      94 271
Fragmentation, under EI conditions      4
Frit nebulizers      146
Gas chromatography (GC)      4 77 245
Gas chromatography (GC), analyzers, coupling of to mass spectrometers      252
Gas chromatography (GC), detectors, sensitivity of      252
Gas chromatography (GC), development of      253
Gas chromatography (GC), mass chromatogram      298
Gas chromatography (GC), peak, scanning of mass spectrum over      256
Gas chromatography (GC), retention-time accuracy      300
Gas chromatography (GC), separation by      74
Gas chromatography and liquid chromatography      245—252
Gas chromatography and liquid chromatography, chromatographic process      248—250
Gas chromatography and liquid chromatography, detectors      250—251
Gas chromatography and liquid chromatography, injectors      250
Gas chromatography and liquid chromatography, principles of gas and liquid chromatography      245—246
Gas chromatography and liquid chromatography, requirements for chromatographic apparatus      246—247
Gas chromatography and liquid chromatography, typical stationary phases for use in      248
Gas chromatography and liquid chromatography, uses of GC and LC      251—252
Gas chromatography/mass spectrometry (GC/MS)      253—260
Gas chromatography/mass spectrometry (GC/MS), advantage of magnetic instrument in      256
Gas chromatography/mass spectrometry (GC/MS), connection between GC and MS      254—255
Gas chromatography/mass spectrometry (GC/MS), instruments, output from      324
Gas chromatography/mass spectrometry (GC/MS), manipulation of scan data      257—260
Gas chromatography/mass spectrometry (GC/MS), recording mass spectra      255—257
Gas chromatography/mass spectrometry (GC/MS), sample analysis by      296
Gas chromatography/mass spectrometry (GC/MS), systems, ion sources in      254
Gas chromatography/mass spectrometry (GC/MS), use of CI/EI in tandem in      4
Gas, argon      89 90 152
Gas, atoms, ionization of neutral      42
Gas, background      374
Gas, bath      282 378
Gas, carrier      152
Gas, chromatograms      247 257 259
Gas, collision      74 161 374
Gas, diffusion      95
Gas, direct heating of      87
Gas, drying      62 63
Gas, electric discharges in      30
Gas, electromagnetically heated      91
Gas, fast-flowing      142
Gas, flow, capillary GC column      101
Gas, flow, effect of on discharge      38
Gas, helium as background      374
Gas, inlet      276
Gas, introduction of      98 101
Gas, lasers      131
Gas, liquid chromatography (GLC)      245
Gas, pressure, effect of on discharge      38
Gas, pressure, ion/molecule collisions and      372
Gas, reagent      2 3
Gas, state lasers      129
GC      see “Gas chromatography”
GC/MS      see “Gas chromatography/mass spectrometry”
Gel-filtration chromatography      331
Gene, cloning      328
Gene, machine      328 329
genetic engineering      328 334
Glass, refractive index of      128
GLC      see “Gas liquid chromatography”
Glow, anode      34 35
Glow, discharge, characteristics      39
Glow, discharge, colors of light emitted in different regions of      33
Glow, discharge, electric-field gradients across      35
Glycerol, as matrix      85
Gold plating, on ceramic      12
Grass      86
Ground states, populations of      124
Guanine      327
Guided motion      380
Guiding potential      379
Hall-effect probe      242
Halo compounds      5
Hb Montreal — Chori      292
Heating, electrical      114
Heavy water      353
Helium, as background gas      374
Helium, atom(s), excited-state      131
Helium, atom(s), formation of      132
Hemoglobin, electrospray mass spectrum of      58
Hemophilia, use of DNA sequence data to investigate      329
HEN      see “High-efficiency nebulizer”
Hexapole time-of-flight instruments, advantages of hybrid      167
Hexapole time-of-flight instruments, hexapole bridge      164—165
Hexapole time-of-flight instruments, hybrid      163—167
Hexapole time-of-flight instruments, inlet systems      163—164
Hexapole time-of-flight instruments, operation of hybrid      166—167
Hexapole time-of-flight instruments, time-of-flight analyzer      165—166
Hexapole(s), /TOF instrument      164
Hexapole(s), assembly      170
Hexapole(s), bridge      164
Hexapole(s), connection of rods in      381
Hexapole(s), unit, diagrammatic representation of      165
Hexapole(s), use of in commercial instruments      382
High-efficiency nebulizer (HEN)      143
High-performance liquid chromatography (HPLC)      61 77 268
HPLC      see “High-performance liquid chromatography”
Hybrid analyzers      153
Hybrid instruments      281
Hybrid operation      166
Hydrides, analysis of elemental      99
Hydrides, borohydride method of forming volatile      100
Hydrides, generation of volatile      98 99
Hydrogen-bonding forces      279
iCR      see “Ion cyclotron resonance”
Immune response      334
In-line analyzers      153
Incandescent lamp      120 121
Inductively coupled plasma atomic emission spectroscopy (ICP/AES)      87—88 97
Inductively coupled plasma mass spectrometry (ICP/MS)      87 97
Inductively coupled plasma mass spectrometry (ICP/MS), charged droplets in      151
Inductively coupled plasma mass spectrometry (ICP/MS), examination of samples by      103 109 137
Inductively coupled plasma mass spectrometry (ICP/MS), examination of solutions by      108
Inductively coupled plasma mass spectrometry (ICP/MS), instrument, GC connections to      101
Inductively coupled plasma mass spectrometry (ICP/MS), instrument, solutions introduced into      107
Inductively coupled plasma mass spectrometry (ICP/MS), nebulizers used in      139
Inductively coupled plasma mass spectrometry (ICP/MS), use of laser for ablative sampling in      112
Inlet(s), liquid      104
Inlet(s), nebulization      108
Inlet(s), target, line-of-sight trajectory to      56
Inlet(s), trajectories for      67
Inlet(s), tube sprays, normal      66
Inlet(s), Z-spray      69
Instrument(s), control      320
Instrument(s), design      371
Instrument(s), GC/MS, output from      324
Instrument(s), LC/MS, output from      324
Instrument(s), use of quadrupoles and hexapoles in commercial      382
Instrument(s), well-tuned      321
Interference devices      119
International units, system of      361
1 2 3 4 5 6
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