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Katz E. (ed.) Ч Handbook of HPLC
Katz E. (ed.) Ч Handbook of HPLC

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Ќазвание: Handbook of HPLC

јвтор: Katz E. (ed.)

јннотаци€:

Discusses principles, techniques, and instrumentation involving HPLC, delineating its usage in separation, purification, and detection processes across a wide variety of disciplines in industry and research. Part I covers HPLC theory, and Part II discusses different HPLC modes and critically addresses their applicability and limitations. Part III describes principles and practical operations of modern HPLC equipment, and Part IV examines applications. For chemists, biologists, and students.


язык: en

–убрика: “ехнологи€/

—татус предметного указател€: √отов указатель с номерами страниц

ed2k: ed2k stats

√од издани€: 1998

 оличество страниц: 974

ƒобавлена в каталог: 18.02.2007

ќперации: ѕоложить на полку | —копировать ссылку дл€ форума | —копировать ID
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ѕредметный указатель
$\alpha$-olefin sulfonates      793
$\alpha$-olefin sulfonates other anionic sulfonates      793Ч795
$\alpha_1$-Acidglycoprotein (ACP) chiral stationary phase      673Ч675
6-Methylen-androsta-l,4-diene-3,7-dione      654
Acid-base equilibria      37Ч47
Acrylic polymer-based phase for ion-exchange chromatography      386Ч387
Actinides      820Ч821
Activity coefficients in mixed liquid phases      7Ч14
Acyclovir      630
Adsorption chromatography      325Ч348
Adsorption chromatography retention mechanisms      327Ч348
Adsorption chromatography retention mechanisms, applications      344Ч348
Adsorption chromatography retention mechanisms, localized and delocalized interactions      329
Adsorption chromatography retention mechanisms, main parameters goveming solutes      329Ч340
Adsorption chromatography retention mechanisms, mobile phase choice and optimization      340Ч344
Adsorption chromatography retention mechanisms, Snyder Ч Soczewkinski model      327Ч329
Adsorption chromatography stationary phases      325Ч327
Adsorption chromatography stationary phases, bare silica      325Ч327
Adsorption chromatography stationary phases, miscellaneous adsorbents      327
Adsorption isotherms determination by displacement chromatography      883Ч885
Advanced data analysis, computer-assisted      259Ч267
Affinity chromatography (AFC)      483Ч498
Affinity chromatography (AFC) principles      483Ч491
Affinity chromatography (AFC) principles, application conditions      489Ч491
Affinity chromatography (AFC) principles, elution conditions      491
Affinity chromatography (AFC) principles, immobilization methods      489 490
Affinity chromatography (AFC) principles, support materials      487Ч489
Affinity chromatography (AFC) principles, theoretical basis      484Ч486
Affinity chromatography (AFC) principles, types of affinity ligands      486Ч487
Affinity chromatography (AFC) stationary phases      32Ч33
Affinity chromatography (AFC) types of AFC      492Ч496
Affinity chromatography (AFC) types of AFC analytical affinity chromatography      495Ч496
Affinity chromatography (AFC) types of AFC bioaffinity chromatography      492
Affinity chromatography (AFC) types of AFC dye-ligand affinity chromatography      494
Affinity chromatography (AFC) types of AFC immobilized metal ion affinity chromatography      494Ч495
Affinity chromatography (AFC) types of AFC immunoaffinity chromatography      492Ч494
Affinity chromatography (AFC) types of AFC miscellaneous ligands and methods      496
Agricultural applications of biotechnology      696
Alclofenac      630Ч631
Alcohol ethoxylates      801
Alcohols, dervatization of      684Ч685
Alkali metals      818
Alkaline earth metals      818
Alkanesulfonates      790Ч791
Alkyl sulfates      790Ч791
Alkylarylsulfonates      791Ч792
Alkylphenol ethoxylates      800Ч801
Alumina      22 24
Alumina, adsorption chromatography and      327
Alumina, chemically bonded alumina-based phases      315
Alumina, polymer-coated alumina-based phases      316
Amfenac      631
Amine oxides      802
Amines, denvatization of      685Ч686
Amino acids      707Ч716
Amino acids classic analysis of      707
Amino acids detection of underivatized ammo acids      709
Amino acids hydrolysis of polypeptides      707Ч709
Amino acids postcolumn reaction detection methods      709Ч710
Amino acids precolumn denvatization techniques      710Ч716
Ammonium      821
Amoxicillin      631Ч632
Amphoteric surfactants      796Ч798
Analytical affinity chromatography      495Ч496
Analytical affinity chromatography, ion-exchange process for low molecular weight ions in      366Ч371
Anion self-regenerating suppressor      428 429
Anion separation in nonsuppressed ion chromatography      441
Anionic surfactants      790Ч795
Anionic surfactants alkyl sulfates and alkanesulfonates      790Ч791
Anionic surfactants alkylarylsulfonates      791Ч792
Anionic surfactants ether sulfates      792Ч793
Anions      see УIons and inorganic speciesФ
Arsenic anions      815Ч816
Art conservation      903Ч927
Art conservation, background      903Ч904
Art conservation, future applications      919Ч920
Art conservation, future applications fatty acid analysis and hybrid techniques      919Ч920
Art conservation, future applications LC-mass spectrometry      920
Art conservation, future applications, carbohydrate analysis of gums and celluloses      919
Art conservation, general areas of investigation      904Ч905
Art conservation, primary HPLC applications      905Ч919
Art conservation, primary HPLC applications, identification of natural and early synthetic dyestuffs      905Ч909
Art conservation, primary HPLC applications, ion chromatography for monitoring inorganic contaminants      918
Art conservation, primary HPLC applications, monitoring organic pollutants in museum environment      918Ч919
Art conservation, primary HPLC applications, proteinaceous materials in conservation      910Ч914
Art conservation, primary HPLC applications, study of degradation and polymerization reactions      914Ч918
Ascorbic acid      632
Atmospheric pressure chemical ionization (APCI) process      591Ч593 960Ч964
Atomic absorption (AA)      404Ч406
Atomic absorption (AA), LC-atomic absorption spectroscopy (LC-AA) tandem systems      596Ч600
Autosamplers      569 570Ч571
BAYy3118      632
Benorylate, quantitation of impurities in      356Ч357 358
Bioaffinity chromatography      492
Biological ion exchangers      390Ч391
Biologically active compounds      see УDrugs in biological samplesФ
Biomedical science, role of hydrophobicity in      860Ч861
biotechnology      695Ч751
Biotechnology amino acids      707Ч716
Biotechnology amino acids, classic analysis      707
Biotechnology amino acids, detection of underivatized amino acids      709
Biotechnology amino acids, hydrolysis of polypeptides      707Ч709
Biotechnology amino acids, postcolunm reaction detection methods      709Ч710
Biotechnology amino acids, precolumn derivatization techniques      710Ч716
Biotechnology carbohydrates      734Ч742
Biotechnology carbohydrates complex carbohydrates      736Ч739
Biotechnology carbohydrates microheterogeneity of glycoproteins      739Ч742
Biotechnology carbohydrates simple carbohydrates and related compounds      735Ч736
Biotechnology downstream processing      742Ч745
Biotechnology general chromatographic developments      700Ч707
Biotechnology general chromatographic developments, bioprocess control      700Ч702
Biotechnology general chromatographic developments, column technology      702Ч707
Biotechnology methodology      697Ч700
Biotechnology nucleic acid and related compounds      729Ч734
Biotechnology nucleic acid and related compounds, large deoxyribonucleotides      732Ч733
Biotechnology nucleic acid and related compounds, large ribonucleotides      733Ч734
Block copolymers of ethylene oxide and propylene oxide      802
Bromazepam      633
Bulk properly detectors      536Ч539
Bulk properly detectors electrical conductivity detector      537Ч539
Bulk properly detectors refractive index detectors      536Ч537
Buprenorphine      634
Calibration for an SEC system      277Ч281
Calibration for an SEC system broad-molecular weight calibration      279
Calibration for an SEC system primary calibration      278
Calibration for an SEC system secondary calibration      279
Calibration for an SEC system universal calibration      279Ч281
Canrenone      635
Capillary electrophoresis (CE)      44Ч46 169Ч191 822Ч824
Capillary electrophoresis (CE), emergence of commercial instruments      170Ч172
Capillary electrophoresis (CE), HPLC and      170
Capillary electrophoresis (CE), modes      184Ч189
Capillary electrophoresis (CE), modes capillary gel electrophoresis      188Ч189
Capillary electrophoresis (CE), modes capillary isolectic focusing      187Ч188
Capillary electrophoresis (CE), modes capillary isotachophoresis      186Ч187
Capillary electrophoresis (CE), modes capillary zone electrophoresis      185Ч186
Capillary electrophoresis (CE), modes micellar electrokinetic capillary chromatography      186
Capillary electrophoresis (CE), principles      172Ч184
Capillary electrophoresis (CE), principles, electro osmotic flow      174Ч177
Capillary electrophoresis (CE), principles, electrophoresis mobility      172Ч173
Capillary electrophoresis (CE), principles, experimental considerations      182Ч184
Capillary electrophoresis (CE), principles, factors influencing performance      180Ч182
Capillary electrophoresis (CE), principles, separation efficiency and resolution      177Ч180
Capillary gel electrophoresis (CGE)      170 188Ч189
Capillary isolectric focusing (CIEF)      170 187Ч188
Capillary zone electrophoresis (CZE)      170 185Ч186
Carbamazepine      635
Carbohydrate analysis of gums and cellulose      919
Carbohydrates      734Ч742 753Ч757
Carbohydrates, complex carbohydrates      736Ч739
Carbohydrates, microheterogeneity of glycoproteins      739Ч742
Carbohydrates, simple carbohydrates and related compounds      735Ч736
Carbon-based phases for RPLC      314
Carbon-clad zirconia      316
Carboxylic acids      817
Carboxylic acids derivatization of      686Ч687
Catecholamines      636Ч638
Cation self-regenerating suppressor      428 429
Cationic surfactants      795
Cations      see УIons and inorganic speciesФ
Celiprolol      638
Cellulose-based phases      387Ч391
Check valves      505Ч508
Chelation equilibria      49Ч51
Chemically bonded alumina-based phases      315
Chemically bonded silica-based phases for RPLC      298Ч310
Chemically bonded silica-based phases for RPLC, characterization techniques      308Ч310
Chemically bonded silica-based phases for RPLC, monomeric stationary phases      299Ч302
Chemically bonded silica-based phases for RPLC, polymeric stationary phases      302
Chemically bonded silica-based phases for RPLC, selectivities of phases      303Ч308
Chemicals, application of biotechnology for      696
Chemisorption chromatography      496
Chiral pharmaceutical analysis      669Ч693
Chiral pharmaceutical analysis, chiral mobile-phase additives (CMPAs)      677Ч682
Chiral pharmaceutical analysis, chiral mobile-phase additives (CMPAs), chiral counterions      678Ч680
Chiral pharmaceutical analysis, chiral mobile-phase additives (CMPAs), cyclodextrins      680Ч682
Chiral pharmaceutical analysis, chiral mobile-phase additives (CMPAs), ligand- exchange chromatography      678
Chiral pharmaceutical analysis, chiral stationary phases (CSPs)      670Ч677
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), $\alpha_1$-acidglycoprotein      673Ч675
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), cyclodextrin stationary phases      675Ч676
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), ovomucoid-bonded stationary phase      675
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), Pirkle phases      677
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), polysaccharides      670Ч673
Chiral pharmaceutical analysis, chiral stationary phases (CSPs), serum albumin phases      675
Chiral pharmaceutical analysis, enantioselectivity in biological systems      669
Chiral pharmaceutical analysis, indirection separation of enantiomers      682Ч687
Chiral pharmaceutical analysis, indirection separation of enantiomers derivatization of alcohol      684Ч685
Chiral pharmaceutical analysis, indirection separation of enantiomers derivatization of amines      685Ч686
Chiral pharmaceutical analysis, indirection separation of enantiomers derivatization of carboxylic acids      686Ч687
Chiral pharmaceutical analysis, separation of enantiomers by HPLC      670
Chiral stationary phases (CSPs)      33Ч35 670Ч677
Chloroguanide      638
Chloroqume      638
Chlortetracycline      666
Chlorzoxazone      638Ч639
Chromate      816
Chromatographic hydrophobicily index      867Ч873
Chromatographic profiles and retention, prediction of      238Ч246
Chromatographic profiles and retention, prediction of quantitative structure-retention relations      241Ч243
Chromatographic profiles and retention, prediction of simulation of profiles      240Ч241
Chromatographic profiles and retention, prediction of Уfirst-guessФ expert systems      243Ч246
Clobazam      639
Clozapine      639
Cocaine      639Ч641
Collection devices      617Ч627
Collection devices applications      622
Collection devices fraction collectors      617Ч618
Collection devices operational considerations of fraction collection      618Ч622
Collection devices operational considerations of fraction collection low-resolution techniques      618
Collection devices operational considerations of fraction collection separation of complex mixtures      618Ч622
Collection devices other types of fraction collection devices      622Ч625
Collection devices troubleshooting      625Ч627
Column efficiency, effects of temperature on      608
Column-switching methods      198Ч205
Column-switching methods, effects of the column in LC      198Ч200
Column-switching methods, relative advantages and disadvantages of gradient-elution LC methods and      230
Column-switching methods, relative advantages and disadvantages of isocratic LC separations and      229
Column-switching methods, valve-switching options and requirements      200Ч205
Column-switching valves      569Ч573
Complex carbohydrates      736Ч739
Complex stability constants, determination of      875Ч878
Complexation equilbna      47Ч51
Compressibility effects onflow and plate weight      118Ч120
Computers      233Ч271
Computers, advanced data analysis      259Ч267
Computers, advanced data analysis, multivariate data analysis      263Ч267
Computers, advanced data analysis,univariate data analysis      260Ч263
Computers, automation and instrument control      234Ч238
Computers, automation and instrument control, column coupling and hyphenated separation techniques      237Ч238
Computers, automation and instrument control, on-line monitoring and control      238
Computers, automation and instrument control, sample preparation      235Ч237
Computers, computer-assisted method development      246Ч257
Computers, computer-assisted method development for gradient separations      253Ч255
Computers, computer-assisted method development for isocratic separations      255Ч257
Computers, computer-assisted method development, general considerations      247Ч251
Computers, computer-assisted method development, optimization criteria      251Ч252
Computers, interlaboratory tests using on-line LC      964Ч970
Computers, method validation      257Ч259
Computers, prediction of chromatographic profiles and retention      238Ч246
Computers, prediction of chromatographic profiles and retention, quantitative structure-retention relations      241Ч243
Computers, prediction of chromatographic profiles and retention, simulation of profiles      240Ч241
Computers, prediction of chromatographic profiles and retention, Уfirst-guessФ expert systems      243Ч246
Conductimetric detection      395Ч396
Conductivity detection      160Ч162
Conductivity detection in ion chromatography      417Ч419
Conductivity detection principles of operation      160Ч161
Conductivity detection suppression systems      161Ч162
Constant flow rate pumps      500Ч501
Constant-pressure pumps      500
Cosmetics, applications of biotechnology for      696
Coumann      641Ч642
Cyclamates      754
Cyclodextrins (CDs)      680Ч682
Danazol      642
Debrisoquine      642
Deoxyribonucleotides, large      732Ч733
Detectors (detection)      143Ч168 531Ч558
Detectors (detection) as operating variable in ion-exchange chromatography      395Ч406
Detectors (detection) in ion interaction chromatography      457Ч459
Detectors (detection) to identify lipid components      758Ч761 764 765 766
Detectors (detection), bulk properly detectors      536Ч539
Detectors (detection), bulk properly detectors, electrical conductivity detector      537Ч538
Detectors (detection), bulk properly detectors, refractive index detectors      536Ч537
Detectors (detection), choice of detectors      555Ч556
Detectors (detection), comparison of detector performances      167Ч168
Detectors (detection), conductivity detection      160Ч162
Detectors (detection), conductivity detection principles of operation      160Ч161
Detectors (detection), conductivity detection suppression systems      161Ч162
Detectors (detection), derivatization      554Ч555
Detectors (detection), detectors for polymer analysis      162Ч165
Detectors (detection), detectors for polymer analysis, evaporative detectors      163Ч164
Detectors (detection), detectors for polymer analysis, light-scattering detection      164Ч165
Detectors (detection), detectors for polymer analysis, viscosity detectors      165
Detectors (detection), effects of temperature on      609Ч610
Detectors (detection), electrochemical detection      156Ч160
Detectors (detection), electrochemical detection, electrode materials, flow-cells, and instrumentation      158
Detectors (detection), electrochemical detection, principles of operation      156Ч158
Detectors (detection), electrochemical detection, pulsed-amperometric detection      159Ч160
Detectors (detection), electrochemical detection, selectivity enhancement      159
Detectors (detection), fluorescence detection      150Ч154
Detectors (detection), fluorescence detection, fluorescence yields      152
Detectors (detection), fluorescence detection, instrumentation      152Ч153
Detectors (detection), fluorescence detection, postcolunm denvatization      154
Detectors (detection), fluorescence detection, precolunm fluorescence labeling      153
Detectors (detection), for the SEC system      284Ч289
Detectors (detection), for the SEC system, composition detectors      285Ч287
Detectors (detection), for the SEC system, concentration detectors      284Ч285
Detectors (detection), for the SEC system, molecular-weight-sensitive detectors      287Ч289
Detectors (detection), operation of LC detectors      556
Detectors (detection), other detectors      165Ч167
Detectors (detection), other detectors, gas-phase detectors      167
Detectors (detection), other detectors, infrared detection      165Ч166
Detectors (detection), other detectors, optical activity detection      166
Detectors (detection), other detectors, radiochemical detection      166
Detectors (detection), refractive index detection      154Ч156
Detectors (detection), refractive index detection, optical principles      155
Detectors (detection), refractive index detection, performance and application      156
Detectors (detection), requirements for and characterization of detectors      143Ч147
Detectors (detection), requirements for and characterization of detectors, linearity      146
Detectors (detection), requirements for and characterization of detectors, peak broadening      144
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