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Katz E. (ed.) Ч Handbook of HPLC
Katz E. (ed.) Ч Handbook of HPLC



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Ќазвание: Handbook of HPLC

јвтор: Katz E. (ed.)

јннотаци€:

Discusses principles, techniques, and instrumentation involving HPLC, delineating its usage in separation, purification, and detection processes across a wide variety of disciplines in industry and research. Part I covers HPLC theory, and Part II discusses different HPLC modes and critically addresses their applicability and limitations. Part III describes principles and practical operations of modern HPLC equipment, and Part IV examines applications. For chemists, biologists, and students.


язык: en

–убрика: “ехнологи€/

—татус предметного указател€: √отов указатель с номерами страниц

ed2k: ed2k stats

√од издани€: 1998

 оличество страниц: 974

ƒобавлена в каталог: 18.02.2007

ќперации: ѕоложить на полку | —копировать ссылку дл€ форума | —копировать ID
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ѕредметный указатель
Ions and inorganic species, chromatographic methods for cationic species lanthanides and actinides      820Ч821
Ions and inorganic species, chromatographic methods for cationic species noble metals      820
Ions and inorganic species, chromatographic methods for cationic species transition metals      819Ч820
Ions and inorganic species, HPLC analysis of inorganic species in specific industries      822
Ions and inorganic species, methods for common anion mixtures      810Ч813
Ions and inorganic species, methods for specific anionic species      813Ч817
Ions and inorganic species, methods for specific anionic species arsenic, selenium, and tellurium anions      815Ч816
Ions and inorganic species, methods for specific anionic species carboxylic acids      817
Ions and inorganic species, methods for specific anionic species halides, pseudohalides, and oxyhalides      813Ч814
Ions and inorganic species, methods for specific anionic species inorganic complexes      816
Ions and inorganic species, methods for specific anionic species miscellaneous inorganic anions      816
Ions and inorganic species, methods for specific anionic species molybdate, tungstate, and chromate      816
Ions and inorganic species, methods for specific anionic species nitrogen-containing anions      814
Ions and inorganic species, methods for specific anionic species phosphorus-containing anions      815
Ions and inorganic species, methods for specific anionic species sugars      817
Ions and inorganic species, methods for specific anionic species sulfur-containing anions      814Ч815
Ions and inorganic species, separation of      805Ч810
Ions and inorganic species, separation of organometallic compounds      821
Ions and inorganic species, separation of, modes of separation      806Ч807
Ions and inorganic species, separation of, practical aspects of ion chromatographic separations      807Ч81
Ions and inorganic species, separation of, sample pretreatment      809Ч810
Ions and inorganic species, simultaneous determination of anions and cations      822
Isocratic elution      499Ч510
Isocratic elution, comparison of column-switching LC separations and      229
Isocratic elution, comparison of gradient-elution LC separations and      227
Isocratic elution, computer-assisted methods for isocratic separations      255Ч257
Isocratic elution, constant flow rate pumps      500Ч501
Isocratic elution, constant-pressure pumps      500
Isocratic elution, flow programming      509
Isocratic elution, reciprocating pumps      501Ч508
Isocratic elution, recycle chromatography      510
Isocratic elution, syringe pumps      509
Isocratic elution, troubleshooting      519Ч520
Isotachophoresis (ITP)      170 186Ч187
Iterative target-transformation factor analysis (ITT-FA)      267
Kinetic optimization      123Ч133
Kinetic optimization of separation methods for macromolecules      133Ч140
Kinetic optimization of separation methods for macromolecules, compressible supercritical Kinetic optimization of separation methods for macromolecules, fluid chromatographic methods      134Ч136
Kinetic optimization of separation methods for macromolecules, field-flow fractionation      140
Kinetic optimization of separation methods for macromolecules, hydrodynamic chromatography      138Ч140
Kinetic optimization of separation methods for macromolecules, SEC      136Ч138
Kinetic optimization particle size limitations      127Ч129
Kinetic optimization pressure limitations      125Ч127
Kinetic optimization using reduced variables      129Ч130
Lanthanides      620Ч621
Large deoxyribonucleotides      732Ч733
Large ribonucleotides      733Ч734
Laser desorption mass spectrometry      593Ч596
Ligand-exchange chromatography      678
Ligands in affinity chromatography      486Ч487
Light-scattering detector      164Ч165 285Ч289 551Ч552
Linear-solvent-strength (LSS) model of LC gradients      211Ч214
Lipids      758Ч761
Lipids detectors      758Ч761 764 765 766
Liquid adsorption chromatography (LAC)      850Ч851
Liquid chromatography (LC)-atomic absorption spectroscopy (LC-AAS) tandem systems      596Ч600
Liquid chromatography with diode-array detection (LC-DAD)      940Ч941
Liquid chromatography with electrochemical detection (LC-ECD)      941Ч944
Liquid chromatography with fluorescence detection (LC-FD)      945
Liquid chromatography-infrared (LC-IR) tandem systems      600Ч602
Liquid chromatography-mass spectrometry (LC-MS) tandem systems      585Ч596
Liquid chromatography-mass spectrometry (LC-MS) tandem systems atmospheric ionization interface      591Ч593
Liquid chromatography-mass spectrometry (LC-MS) tandem systems electro spray interface      589Ч591 953Ч960
Liquid chromatography-mass spectrometry (LC-MS) tandem systems in analysis of organic pollutants in water      945Ч964
Liquid chromatography-mass spectrometry (LC-MS) tandem systems in analysis of organic pollutants in water, with atmospheric pressure chemical ionization      960Ч964
Liquid chromatography-mass spectrometry (LC-MS) tandem systems in analysis of organic pollutants in water, with ionspray interface      953Ч960
Liquid chromatography-mass spectrometry (LC-MS) tandem systems in analysis of organic pollutants in water, with thermospray interface      945Ч953
Liquid chromatography-mass spectrometry (LC-MS) tandem systems in art conservation      920
Liquid chromatography-mass spectrometry (LC-MS) tandem systems laser desorption mass spectrometry      593Ч596
Liquid chromatography-mass spectrometry (LC-MS) tandem systems thermospray interface      587Ч589 945Ч953
Liquid chromatography-mass spectrometry (LC-MS) tandem systems transport interface      586Ч587
Liquid chromatography-nuclear magnetic resonance (LC-NMR) tandem systems      602Ч604 605
Liquid precipitation chromatography (LPC)      852
Liquid-liquid chromatography (LLC)      1
Liquid-liquid chromatography (LLC) distribution equilibria in      7Ч14
Liquid-liquid chromatography (LLC) in extracting organic pollutants from water      931Ч932
Liquid-solid chromatography (LSC)      1
Liquid-solid chromatography (LSC) distribution equilibria in      7Ч14
Liquid-solid chromatography (LSC) in extracting organic pollutants from water      932Ч940
Lisuride      652Ч653
Low-angle laser-light-scattering (LALLS) detectors      164Ч165
Low-dispersion connecting tubes      582Ч586
Macromolecular chromatography, kinetic optimization of separation methods for      133Ч140
Macromolecular chromatography, kinetic optimization of separation methods for compressible supercritical fluid chromatographic methods      134Ч136
Macromolecular chromatography, kinetic optimization of separation methods for field-flow fractionation      140
Macromolecular chromatography, kinetic optimization of separation methods for hydrodynamic chromatography      138Ч140
Macromolecular chromatography, kinetic optimization of separation methods for SEC      136Ч138
Manual sample injection valves      559Ч568
Manual sample injection valves sample-loading techniques      563Ч566
Manual sample injection valves small-volume sample injection      566Ч563
Mass spectrometiy (MS)      286 400Ч404
Mass spectrometiy (MS) laser desorption MS      593Ч596
Matrix-assisted laser desorption mass spectrometry (MALDI-MS)      595
MDL 73,005EF (binspirone mesylate)      653Ч654
Mechanisms of zone-broadening      69Ч107
Mechanisms of zone-broadening, alternative expressions and additional forms of broadening      82Ч107
Mechanisms of zone-broadening, convective dispersion in the mobile phase      71Ч79
Mechanisms of zone-broadening, longitudinal molecular diffusion      69Ч70
Mechanisms of zone-broadening, sorption and desorption      80Ч82
Medical applications of biotechnology      696
Membrane proteins      726Ч728
Metal oxide supports in RPLC      314Ч317
Metal oxide supports in RPLC chemically bonded alumina-based phases      315
Metal oxide supports in RPLC polymer-coated alumina-based phases      316
Metal oxide supports in RPLC zirconia- and titania-based phases      316Ч317
Metoclopramide      654Ч655
Micellar electrokinetic chromatography (MEKC)      51Ч52 170 186
Microcapillary hydrodynamic chromatography (MHDC)      138
Microheterogeneity of glycoproteins      739Ч742
Micromembrane suppressor (MMS)      424Ч427
Midazolam      647Ч648
Minerals      761Ч762 763 768Ч774
Mitomycin      655
Mizolastine      655^
Mobile phases of hydrophobic interaction chromatography      472Ч473
Mobile-phase delivery systems      499Ч529
Mobile-phase delivery systems, biocompatability and materials of construction      513Ч516
Mobile-phase delivery systems, flow rate range      516Ч517
Mobile-phase delivery systems, gradient elution      510Ч512 513
Mobile-phase delivery systems, gradient elution problems, causes, and remedies in multipump gradient elution      514
Mobile-phase delivery systems, gradient elution troubleshooting      521Ч522
Mobile-phase delivery systems, isocratic elution      499Ч510
Mobile-phase delivery systems, isocratic elution constant flow rate pumps      500Ч501
Mobile-phase delivery systems, isocratic elution constant-pressure pumps      500
Mobile-phase delivery systems, isocratic elution flow programming      509
Mobile-phase delivery systems, isocratic elution reciprocating pumps      501Ч508
Mobile-phase delivery systems, isocratic elution recycle chromatography      510
Mobile-phase delivery systems, isocratic elution syringe pumps      509
Mobile-phase delivery systems, isocratic elution troubleshooting      519Ч520
Mobile-phase delivery systems, pulse dampers      517Ч518
Mobile-phase delivery systems, pump table      523Ч528
Mobile-phase delivery systems, troubleshooting      518Ч522
Molecular-weight-sensitive detectors for SEC systems      287Ч289
Molecular-weight-sensitive detectors for SEC systems, light-scattering detection      288Ч289
Molecular-weight-sensitive detectors for SEC systems, light-scattering viscometry      289
Molecular-weight-sensitive detectors for SEC systems, viscosity      287Ч288
Molybdate      816
Morphine      655Ч656
Multiangle laser-light-scattering (MALLS) detector      165
Multiple wavelength absorbance detection      149Ч150
Multipump gradient elutions, problems, causes, and remedies in      514
Multivariate data analysis, computer-assisted      263Ч261
Natural dye stuffs, identification of      905Ч909
Nicorandil      656
Nicotine      656Ч657
Nifedipine      657
Nitrogen-containing anions      814
Noble metals      820
Nonionic surfactants      799Ч802
Nonionic surfactants, analysis of individual surfactants      800Ч802
Nonionic surfactants, general principles      799Ч800
Nonsuppressed ion chromatography      440Ч448
Nonsuppressed ion chromatography, detection by postcolumn reaction      445Ч448
Nonsuppressed ion chromatography, eluent counterion      441Ч444
Nonsuppressed ion chromatography, nonsuppression      440Ч441
Norbuprenorphine      634
Normal-phase (NP) liquid chromatography      325Ч363
Normal-phase (NP) liquid chromatography, adsorption chromatography      325Ч348
Normal-phase (NP) liquid chromatography, adsorption chromatography, retention mechanisms      327Ч348
Normal-phase (NP) liquid chromatography, adsorption chromatography, stationary phases      325Ч327
Normal-phase (NP) liquid chromatography, polar-bonded-phase chromatography      348Ч361
Normal-phase (NP) liquid chromatography, polar-bonded-phase chromatography applications      356Ч361
Normal-phase (NP) liquid chromatography, polar-bonded-phase chromatography bonding reactions      350Ч353
Normal-phase (NP) liquid chromatography, polar-bonded-phase chromatography mobile-phase selection      355Ч356
Normal-phase (NP) liquid chromatography, polar-bonded-phase chromatography retention mechanisms      353Ч355
Normal-phase (NP) liquid chromatography, stationary phases for      26Ч28
Nuclear magnetic resonance (NMR)      286Ч287
Nuclear magnetic resonance (NMR), LC-nuclear magnetic resonance (LCNMR) tandem systems      602Ч604 605
Nucleic acid and related compounds      729Ч734
Nucleic acid and related compounds, large deoxyribonucleotides      732Ч733
Nucleic acid and related compounds, large ribonucleotides      733Ч734
Nucleic acid and related compounds, simple nucleotides      729
Nucleic acid and related compounds, synthetic and small oligodeoxyribonucleotides      729Ч731
Nucleic acid and related compounds, synthetic and small oligoribonucleotides      731Ч732
Oligodeoxyribonucleotides, synthetic and small      729Ч731
Oligomers, separation of      843Ч848
Oligoribonucleotides synthetic and small      731Ч732
On-line LC, interlaboratory tests using      964Ч970
Optical activity detection      166
Optimization of LC conditions, computer-assisted strategies for      251Ч252
Organic amines      821
Organic pollutants in the museum environment, monitoring      918Ч919
Organic pollutants in water      929Ч974
Organic pollutants in water, conventional detectors      940Ч964
Organic pollutants in water, conventional detectors, LC with diode-array detection analysis      940Ч941
Organic pollutants in water, conventional detectors, LC with electrochemical detection      941Ч944
Organic pollutants in water, conventional detectors, LC with fluorescence detection      945
Organic pollutants in water, conventional detectors, LC with mass spectrometric analysis      945Ч964
Organic pollutants in water, interlaboratory tests using on-line LC      964Ч970
Organic pollutants in water, liquid-liquid extractions      931Ч932
Organic pollutants in water, liquid-solid extraction      932Ч940
Organic pollutants in water, sample handling strategies      930Ч940
Organic polymers      24
Organometallic compounds      821
Organosoluble polymers      283
Ovomucoids-bonded stationary phase      675
Oxyhalides      813Ч814
Oxytetracycline      666
Packed-column hydrodynamic chromatography (PHDC)      138
Paclitaxel      657
Partition equilibria      51Ч52
Peptides      720Ч721
Pesticides      776Ч784
pH influence on retention factor and selectivity coefficient      41Ч46
Pharmaceutical applications of biotechnology      696
Phenobarbital      635
Phenolics      767Ч776 777Ч783
Phenytoin      635 658
Phosphorus-containing anions      815
Photodiode array (PDA) detector      761 765
Physic о chemical measurements      855Ч902
Physic о chemical measurements, adsorption isotherms by displacement chromatography      883Ч885
Physic о chemical measurements, determination of equilibrium constants by HPLC      875Ч881
Physic о chemical measurements, determination of equilibrium constants by HPLC, complex stability constants      875Ч878
Physic о chemical measurements, determination of equilibrium constants by HPLC, drug-protein-binding constants      878Ч881
Physic о chemical measurements, determination of hydrophobicity by HPLC      860Ч875
Physic о chemical measurements, determination of hydrophobicity by HPLC, chromatographic hydrophobicity index      867Ч873
Physic о chemical measurements, determination of hydrophobicity by HPLC, determination of partition coefficients      861Ч862
Physic о chemical measurements, determination of hydrophobicity by HPLC, general approach      865Ч867
Physic о chemical measurements, determination of hydrophobicity by HPLC, hydrophobicity in biomedieal sciences      860Ч861
Physic о chemical measurements, determination of hydrophobicity by HPLC, practical aspects      865
Physic о chemical measurements, determination of hydrophobicity by HPLC, theoretical background      862Ч864
Physic о chemical measurements, determination of thermodynamic parameters by HPLC      882Ч885
Physic о chemical measurements, temperature dependence of the retention      882Ч883
Physostigmine      658Ч659
Pirkle phases      677
Polar-bonded-phase chromatography      348Ч361
Polar-bonded-phase chromatography, applications      356Ч361
Polar-bonded-phase chromatography, bonding reactions      350Ч353
Polar-bonded-phase chromatography, mobile-phase selection      355Ч356
Polar-bonded-phase chromatography, retention mechanisms      353Ч355
Poly(styrene)-based phases      385Ч386
Polymer analysis      831Ч858
Polymer analysis, detectors for      162Ч165
Polymer analysis, detectors for evaporative detectors      163Ч164
Polymer analysis, detectors for light-scattering detection      164Ч165
Polymer analysis, detectors for viscosity detectors      165
Polymer analysis, separation by composition      848Ч854
Polymer analysis, separation by composition, separation by liquid adsorption chromatography      850Ч851
Polymer analysis, separation by composition, separation by liquid precipitation chromatography      852
Polymer analysis, separation by composition, separation by other techniques      852Ч854
Polymer analysis, separation by composition, separation mechanisms      849Ч850
Polymer analysis, separation by other functions      854Ч856
Polymer analysis, separation by other functions, field-flow fractionation      855Ч856
Polymer analysis, separation by other functions, temperature-rising elution fractionation      854Ч855
Polymer analysis, separation by size      832Ч848
Polymer analysis, separation by size applications      841Ч843
Polymer analysis, separation by size hydrophobic polymers      848
Polymer analysis, separation by size molecular weight measurements      833Ч841
Polymer analysis, separation by size separation by oligomers      843Ч848
Polymer-based phases for RPLC      312Ч313
Polymer-coated alumina-based phases      316
Polymer-coated silica-based phases for RPLC      310Ч312
Polymer-coated zirconia-based phases      317
Polyols      754
Polypeptides, hydrolysis of      707Ч709
Polysacchande separation employing CSPs      670Ч673
Porous graphitized carbon (PGC)      22 24
Pressure-flow relations in zone spreading      115Ч118
Pressure-flow relations in zone spreading, flow in capillaries      115Ч117
Pressure-flow relations in zone spreading, flow through packed columns      117Ч118
Primidone      635
Programmed analysis      193Ч232
Programmed analysis, column-switching methods      198Ч205
Programmed analysis, column-switching methods, effects of the column in LC      198Ч200
Programmed analysis, column-switching methods, valve-switching options and requirements      200Ч205
Programmed analysis, comparison of main programming methods      226Ч230
Programmed analysis, general elution problem      194Ч195
Programmed analysis, gradient elution      205Ч225
Programmed analysis, gradient elution, gradient optimization      214Ч218
Programmed analysis, gradient elution, gradient scouting      218Ч220
Programmed analysis, gradient elution, gradient solvents      220Ч221
Programmed analysis, gradient elution, instrumental aspects      222Ч225
Programmed analysis, gradient elution, migration under gradient conditions      206Ч211
Programmed analysis, gradient elution, theory of LSS gradients      211Ч214
Programmed analysis, other programming methods      225Ч226
Programmed analysis, other programming methods, ionic-strength programming      226
Programmed analysis, other programming methods, temperature programming in LC      225Ч226
Programmed analysis, place ofprogamming analysis      195Ч198
Propylene oxide, block copolymers of      802
Protein sequencing      716Ч720
Proteinaceous materials in art conservation      910Ч914
Proteins      721Ч728 763Ч767
Proteins general interest      721Ч725
Proteins hydrophobic interaction chromatography of      473Ч479
Proteins immunoglobulins      725Ч726
Proteins membrane proteins      726Ч728
Proteins preparative chromatography of      377Ч381
Pseudohalides      813Ч814
Pulse dampers      517Ч518
Pulsed-amp erometric detection (PAD)      159Ч160 396Ч400
Pump design for isocratic elution constant flow rate pumps      500Ч501
Pump design for isocratic elution constant flow rate pumps constant-pressure pumps      500
Pump design for isocratic elution constant flow rate pumps flow programming      509
Pump design for isocratic elution constant flow rate pumps reciprocating pumps      501Ч508
Pump design for isocratic elution constant flow rate pumps syringe pumps      509
Pyronandine      659Ч660
Quinidine      660
R023-9424      660Ч661
Radio chemical detection      166
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