Lambert J.B., Mazzola E.P. — Nuclear Magnetic Resonance Spectroscopy :: Электронная библиотека попечительского совета мехмата МГУ

Главная Ex Libris Книги Журналы Статьи Серии Каталог Wanted Загрузка ХудЛит Справка Поиск по индексам Поиск Форум

Авторизация

Поиск по указателям

Lambert J.B., Mazzola E.P. — Nuclear Magnetic Resonance Spectroscopy

Обсудите книгу на научном форуме

Нашли опечатку?
Выделите ее мышкой и нажмите Ctrl+Enter

Название: Nuclear Magnetic Resonance Spectroscopy

Авторы: Lambert J.B., Mazzola E.P.

Аннотация:

This book offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. This book focuses on all aspects of NMR including classic methods, modern techniques, practical advice for execution of the NMR experiment, theory, and more. For practicing NMR spectroscopists who want a better understanding of their subject, professors who want a wider knowledge of NMR, preparative (synthetic) organic chemists in industry who want to have more information about how to prove the structures of the compounds they make, and analytical chemists in industry who actually carry out the experiments and want a better understanding of what they are doing.

Язык:

Рубрика: Физика/

Статус предметного указателя: Готов указатель с номерами страниц

ed2k: ed2k stats

Год издания: 2004

Количество страниц: 341

Добавлена в каталог: 21.03.2006

Операции: Положить на полку | Скопировать ссылку для форума | Скопировать ID

Предметный указатель

Solids, spectra of      25—27
Solvent anisotropy      77—78
Solvent anisotropy, effects      see "Medium effects"
Solvent anisotropy, selection      33
Solvent anisotropy, suppression      135 153 204—205
Solvent-solute interactions      78
Spectral analysis      115—119 153—156 204
Spectral analysis, density      317—319
Spectral analysis, editing experiments      see "APT DEPT"
Spectral analysis, subtraction      46 237
Spectral analysis, width, 1D      41—42
Spectral analysis, width, 2D      241—242
Spectral analysis, width, in calibration procedures      58 61
Spectral analysis, width, reduction in the first ( $\nu_{2}$ ) and second ( $\nu_{1}$ ) dimensions      247
Spectrometer components      31—32
Spin      1 21—22 295
Spin locking      27 143 185 198 243 257 266 269 319
Spin locking in HSQC-TOCSY      266
Spin locking in TOCSY      257
Spin locking, sample heating effects      242
spin quantum number      2
Spin rotation relaxation      132 319
Spin tickling      144
Spin wave function      302—303
Spin, angular momentum      295
Spin, decoupling      see "Decoupling"
Spin, diffusion      134 151—152 197—198 321
Spin, echo      153 159 186 204
Spin-diffusion limit      321
Spin-lattice relaxation      10 12 27 44 131—136 143 152 173 192 196 233 297 317—321
Spin-lattice relaxation, time, measurement of      133 233—234 321
Spin-orbit coupling      81 84
Spin-spin relaxation      10 12 26 51 54 134 153 174 180 192 203 297 320
Spin-spin splitting      14 see
Spinner turbine      34
spinning      see "Sample spinning"
Spinning, sidebands      37 39
Spiro[2,5]octane      67
Stacked plot      175
States method of signal detection      241 251 see
Steady-state NOE      237
Steady-state scans, 1D      46 237—238 240
Steady-state scans, 2D      243 251
Steady-state scans, in subtraction experiments      237
Stereochemical descriptors, $\alpha$       292—293
Stereochemical descriptors, $\beta$       292—293
Stereochemistry, from NOE      152
Stereogenic center      103
Steric effects      73—74 76
Stick diagrams      20
Styrene, $^{1}H$ chemical shifts      72
Subtraction artifacts      205
Subtraction experiments, DEPT      236—237 240
Subtraction experiments, NOE difference      238—240
Subtraction experiments, optimizing results      237—238
Sucrose $^{1}H$ spectrum      205—206
Sulfides, $^{13}C$ chemical shifts      84
Sulfides, $^{1}H$ chemical shifts      71
Sulfonic acids, $^{1}H$ chemical shifts      75
Superconducting magnets      see "Magnets"
Symmetric wave function      306—308
Symmetrization      180 250
Symmetry, effect on spectra      280
T-ROESY      198 269
Temperature, performance of 2D experiments at constant      251
Temperature, performance of subtraction experiments at constant      237—238
Tesla      2
Tetramethylsilane      6—7 55
Thiane 1-oxide      123
Three-dimensional NMR      201—203
Through space coupling      114—115
Time domain      13
Time increments in the second ( $\nu_{1}$ ) dimension, with the States method      241 247 251
Time increments in the second ( $\nu_{1}$ ) dimension, with the TPPI method      241

Time scale, NMR      136 336
Time-proportional phase incrementation      241 see
TMS      see "Tetramethylsilane"
Tobey — Simon rule      72—73
TOCSY (1D)      270—272
TOCSY (2D)      184—185 198 207 256—257 283
TOCSY-HMQC      202
Toluene, $^{13}C$ chemical shift      84 87
Toluene, $^{1}H$ chemical shift      71 73
Toluene, anisotropic rotation      134—135
Toluene, isotope effects      79
TPPI      see "Time-proportional phase incrementation"
TQF-COSY      185
trans-2-Butene, $^{13}C$ chemical shift      84 86
trans-2-Butene, $^{1}H$ chemical shift      72
Transition energies      304—305 307—310
Transition probability      306—311
Transmitter      35 58
Transmitter, coils      32
Transmitter, frequency      43
Transmitter, offset in 1D      43
Transmitter, offset in 2D      242
Transverse relaxation      see "Spin-spin relaxation"
Tricyclopentane, $^{1}H- ^{13}C$ coupling constant      105
Trifluoromethyl group, relaxation      320
Tripeptide      177—180
Triple quantum filtration      185
Triple quantum filtration, resonance      143
Truncation      50—51
Truncation of FID's      50—51 54 244
Truncation, artifacts      50—51
Truncation, suppression      50—51
Tubes      see "Sample tubes"
Tumbling frequency      317—318
tuning      see "Probe adjustment"
Two-dimensional NMR experiments      172—232 240—251 328—333
Two-spin system      13
Uncertainty broadening      135—136 321
Valence tautomerization      140—141
van der Waals effect      77—78
van der Waals effect, shielding      68—69
Vanillin, COLOC spectrum      192
Vicinal coupling      17 105 109—112 118 120 124 176 182 189 196 207 214 315
Vinyl acetate, $^{13}C$ spectrum      146—147
Vinyl group      111
Vinyl group, $^{1}H$ chemical shift      72
Virtual coupling      117—118
Volume susceptibility      77
W coupling      114 253 288 see
Wagner — Meerwein rearrangements      141
Waltz      47 58 256 258 262 266 see
WALTZ-16      148 164—165
Water suppression      33
Watergate      204—206
Weighting functions      48—49 244—246
Weighting functions, exponential      48 50
Weighting functions, Gaussian      49
Weighting functions, line broadening      48—49
Weighting functions, resolution enhancement      48—49
Weighting functions, sensitivity enhancement      48 51 246
WURST      258—259 see
X-ray crystallography      1
XCORFE experiment      274
Xylene, inversion recovery stack      168
Xylene, long-range coupling      113
Zeeman effect      2 296—297
Zero filling      49—50 56 58 241 243 246—247 249 251
Zero filling in the first ( $\nu_{2}$ ) and second ( $\nu_{1}$ ) dimensions      241 246—247 251
Zero filling, use in conjunction with linear prediction      249 251
Zero quantum coherence      204 326—327 331—332
Zero referencing, in 1D      55—56
Zero referencing, in 2D      250
Zigzag coupling      114 118 145 193 see
[16]Annulene      65
[18]Annulene      65

1 2 3 4

О проекте