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Lambert J.B., Mazzola E.P. Ч Nuclear Magnetic Resonance Spectroscopy
Lambert J.B., Mazzola E.P. Ч Nuclear Magnetic Resonance Spectroscopy

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Ќазвание: Nuclear Magnetic Resonance Spectroscopy

јвторы: Lambert J.B., Mazzola E.P.

јннотаци€:

This book offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. This book focuses on all aspects of NMR including classic methods, modern techniques, practical advice for execution of the NMR experiment, theory, and more. For practicing NMR spectroscopists who want a better understanding of their subject, professors who want a wider knowledge of NMR, preparative (synthetic) organic chemists in industry who want to have more information about how to prove the structures of the compounds they make, and analytical chemists in industry who actually carry out the experiments and want a better understanding of what they are doing.


язык: en

–убрика: ‘изика/

—татус предметного указател€: √отов указатель с номерами страниц

ed2k: ed2k stats

√од издани€: 2004

 оличество страниц: 341

ƒобавлена в каталог: 21.03.2006

ќперации: ѕоложить на полку | —копировать ссылку дл€ форума | —копировать ID
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ѕредметный указатель
$11\ \beta$-Hydroxyprogesterone, NOE      205Ч206
$AB_{2}$ spectrum      115 312Ч313
$AX_{2}$ spectrum      15 17 100 115 312Ч313
$AX_{4}$ spectrum      17
$AX_{6}$ spectrum      17
$A_{2}$ spectrum      306Ч308 310
$A_{2}B_{2}$ spectrum      339
$A_{2}X$ spectrum      see "$AX_{2}$ spectrum"
$A_{2}X_{2}$ spectrum      100 116Ч117 118 339
$A_{2}X_{3}$ spectrum      16 17 103
$B_{0}$ (static magnetic field)      31 36 295
$B_{0}$ (static magnetic field), effects of inhomogeneity on spectra      37Ч38
$B_{0}$ (static magnetic field), homogeneity      see "Magnetic-field homogeneity"
$B_{0}$ (static magnetic field), optimizing homogeneity      37
$B_{1}$ (radiofrequency magnetic field), calibration      58Ч60
$B_{1}$ (radiofrequency magnetic field), transmitter      31Ч32
$B_{2}$ (double resonance magnetic field), calibration      60Ч61
$B_{2}$ (double resonance magnetic field), decoupler      32
$T_{1}$      see "Spin-lattice relaxation time"
$t_{1}$ noise      180 250 254 259Ч260 263Ч264
$T_{2}$      see "Spin-spin relaxation time"
$T_{2}^{*}$      see "Effective spin-spin relaxation time"
$\alpha$, $\beta$-Unsaturated ketones, $ ^{13}C$ chemical shifts      86
$\alpha$-Thujene      103
$\beta$-Chloroacrylic acid      175Ч176
$\beta$-Chloroacrylic acid, COSY spectrum      175
$\beta$-Methylglutaric acid      117
$\beta$-Quinolmethanol clathrate      26
$\gamma$-Anti effect      83Ч84
$\gamma$-Gauche effect      83
1,1,2-Trichloroethane, $ ^{1}H$ spectrum      15
1,1-Difluoroethene      99Ч101 109
1,1-Dimethylallene, long-range coupling      113
1,2-Dichlorobenzene, $ ^{1}H$ spectrum      101Ч102 123
1,3-Butadiene, long-range coupling      113Ч114
1,3-Cyclohexadicne, $ ^{1}H$ chemical shifts      72
1,3-Cyclohexadicne, HCCH coupling      112
1,3-Cyclopentadiene, $ ^{1}H$ chemical shifts      72
1,3-Cyclopentadiene, HCCH coupling      112
1,3-Dioxane      123
1,4-Cyclohexadiene, homoallylic coupling      113
1,4-Dioxane, isotope effects      79
1-Butene, $ ^{13}C$ chemical shift      86
1-Chloro-2-fluorobenzene      69
1-Chloro-4-nitrobenzene, $ ^{1}H$ spectrum      13Ч14
1-Decanol      168
1-Dehydrotestosterone, $ ^{1}H$ spectrum      145
2,3-Dibromopropionic acid, COSY spectra      181
2-Butyne, long-range coupling      113
2-Chloroethanol, $ ^{1}H$ spectrum      102 316
2-Methylacryloin, allylic coupling      113
3,4-Homotropilidine      140
3-Fluorocamphor      211Ч212
3-Hydroxybutyric acid      12Ч13
3-Hydroxybutyric acid, $ ^{13}C$ spectrum      18 146
3-Methylcyclopropene      100
4-Chlorobenzaldenyde      74
AA'BB' spectrum      101Ч102 116Ч117 136Ч137 315Ч316 339
AA'XX' spectrum      100Ч102 106 115Ч117 315Ч316 339
AB spectrum      98Ч99 115 144 302Ч303 308Ч314
ABC spectrum      111 116 314
Absolute-intensity representation      59 234
Absolute-value representation      183 244 246 250 252
Absorption mode      52Ч53 183Ч185 247 300Ч301 330 see
ABX spectrum      103 105Ч106 111 116Ч117 182 313Ч314
Accordion excitation      275 see modification"
Acetaldehyde, $ ^{13}C$ chemical shift      84 88
Acetaldehyde, $ ^{1}H$ chemical shift      71 73
Acetaldehyde, diethyl acetal      103
Acetaldehyde, HCC coupling      108
Acetamide, $ ^{1}H^{15}N$ coupling constant      106
Acetic acid, $ ^{13}C$ chemical shift      88
Acetic acid, $ ^{1}H$ chemical shift      71 75
Acetone      12Ч13 17 26
Acetone, $ ^{13}C$ chemical shift      84 88
Acetone, $ ^{1}H$ chemical shift      71
Acetone, HCC coupling      108
Acetone, HCH coupling      107
Acetonitrile, $ ^{13}C$ chemical shift      86
Acetonitrile, $ ^{1}H$ chemical shift      71
Acetonitrile, $ ^{1}H- ^{15}N$ coupling constant      106
Acetonitrile, HCH coupling      107
Acetonitrile, NH coupling      167
Acetonitrile, solvent effect      77Ч78
Acetonitrile, vicinal coupling      111
Acetyl chloride $ ^{1}H$ chemical shift      71
acetylene      see "Ethyne"
Acid chlorides, $ ^{13}C$ chemical shifts      88
Acquisition parameters, 1D      39Ч48
Acquisition parameters, 2D      241Ч243
Acquisition time, 1D      42
Acquisition time, 2D      242
Acrolein, dimethyl acetal      194Ч195
Acrylonitrile, $ ^{1}H$ spectrum      111
Active coupling      182 246 254
Adiabatic relaxation      320
Alcohols, $ ^{13}C$ chemical shifts      84
Alcohols, $ ^{1}H$ chemical shifts      70 75
Aldehydes, $ ^{13}C$ chemical shifts      88
Aldehydes, $ ^{1}H$ chemical shifts      73
Aldehydes, shielding      68
Aliasing      40Ч41 see
Aliasing, folded signals      41
Aliasing, noise      46
Alkanes, $ ^{13}C$ chemical shifts      82 85Ч86 89 90
Alkanes, $ ^{1}H$ chemical shifts      69Ч73
Alkanes, vicinal coupling      111Ч112
Alkynes, $ ^{13}C$ chemical shifts      86
Alkynes, $ ^{1}H$ chemical shift      71
Alkynic coupling      113
Allene, long-range coupling      113
Allenes, $ ^{13}C$ chemical shifts      81 88
Allowed transitions      304Ч307
Allylic coupling      112Ч114 282 287Ч288
Alpha effect, on $ ^{13}C$ chemical shifts      82Ч85
Amide bond rotation      137
Amides, $ ^{13}C$ chemical shifts      88
Amides, $ ^{1}H$ chemical shifts      70 76
Amine inversion      139Ч140
Amines, $ ^{13}C$ chemical shifts      84
Amines, $ ^{1}H$ chemical shifts      70 76
Amines, HCN coupling      108
Ammonium ion, $ ^{14}N$ splitting      136
Ammonium ion, $ ^{1}H-N^{15}$ coupling constant      106
Ammonium salts, $ ^{1}H$ chemical shifts      70 76
AMX spectrum      103 106 111 115 182 185Ч186
Angular frequency      3
Angular frequency, methyl group      124
Angular frequency, momentum      1Ч2 80Ч81 296
Anhydrides, $ ^{13}C$ chemical shifts      88
Aniline, $ ^{14}N$ line width      167
Anilines, $ ^{1}H$ chemical shifts      76
Anisochronous      334 339Ч341
Anisole      63 74
Anisotropic rotation      134Ч135
Antiecho experiment      331
Antiphase      156 158 160 163 184 187 189
Antiphase, component      325Ч331
Antisymmetric wave function      310Ч312
Apodization      50Ч51 166 244 246 248
apt      see "Attached proton test"
Aromatic solvent-induced shifts      77Ч79
Aromatics, $ ^{13}C$ chemical shifts      87 90
Aromatics, $ ^{1}H$ chemical shifts      73Ч75
Aromatics, ortho coupling      111
Artifacts, 2D      196Ч197 248 250Ч252 254 259 262 268 269
ASIS      see "Aromatic solvent-induced shifts"
Atomic inversion      139Ч140
Atomic inversion, mass      1Ч2
Attached proton test      155 161 235Ч236
Attached proton test, optimizing sensitivity      235
Autogain feature      45
Average energy of excitation      80
AX spectrum      13Ч14 17 98Ч99 115 148Ч149 162 174Ч175 187 303Ч304 308 310 312
Axial peaks      180 see
Axial peaks, position      66Ч67 83Ч84 110 291Ч292
Axial peaks, protons, relaxation      134
Axial-equatorial interchange      137
Aziridines, nitrogen inversion      139
Barbaralone      141
Baseline correction      54 58
Baseline correction, noise      250
Baseline correction, roll      250
Benzaldehyde, $ ^{13}C$ chemical shift      88
Benzene, $ ^{13}C$ chemical shift      81 86
Benzene, $ ^{1}H$ chemical shift      64 73
Benzene, $ ^{1}H$ spectrum      4 17
Benzene, $ ^{1}H- ^{13}C$ coupling constant      105
Benzene, long-range coupling      113Ч114
Benzene, shielding of      64Ч65 72
Benzene, solvent effect      77Ч78
Benzoquinones      117
Benzylic coupling      113Ч114
Beta effect on $ ^{13}C$ chemical shifts      82Ч85
Biphenyl rotation      138
Bird      189Ч192 258Ч261 265
Bismethylene      315Ч316
Biuret      136
Bloch equations      297Ч301 322
Bloch size      45 243 see
Bloch Ч Siegert shift      146
Boltzmann population      148 151 158
Boltzmann's law      3
Bond anisotropy      67 71
Bond anisotropy, order      81 112
Bond anisotropy, shifts      141Ч142
Boron-11 couplings      106
Branching effect      83Ч84
Broadband decoupling      35 47 146 164 204 242
Bromine relaxation      320Ч321
Bromochloromethane      99Ч100
Bromoethane      99
Brucine, $ ^{1}H$ spectrum      204
Buildup rate      see "NOE"
Bullvalene      141
BURP      166
Butyroacetone      101Ч102
calibrations      58Ч61 237
Calibrations, decoupler pulses      60Ч61
Calibrations, pulse widths      58Ч60
Calicene      138
CAMELSPIN      198
Camphor, HMQC spectrum      189Ч190
Carbocations, shielding      80
Carbon disulfide, solvent effect      77Ч78
Carbon tetrachloride $ ^{35}Cl$ line width      136
Carbon-13 couplings      105Ч106 108 119 121 123 162Ч163 192Ч194 199Ч200
Carbonyl group, shielding      67 72 80
Carbonyl groups, $ ^{13}C$ chemical shifts      88 91
Carboxylic acid, derivatives, $ ^{13}C$ chemical shifts      88
Carboxylic acids, $ ^{1}H$ chemical shifts      68 75
Chair conformation      110 291
Chemical equivalence      99Ч103 106 117Ч118 334Ч335 337
Chemical exchange      136Ч143
Chemical exchange in 2D      195Ч196 198Ч199
Chemical shielding anisotropy      25
Chemical shielding anisotropy, relaxation      132 320
Chemical shift      5Ч8 56 62Ч88 302Ч303
Chemical-shift criterion      102
Chemical-shift difference, AB spectrum      309
Chlorobenzene, relaxation time measurement      133
Chloroform      14
Chloroform, $ ^{13}C$ spectrum      159Ч160
Chloroform, $ ^{1}H$ chemical shift      63
Chloroform, INEPT spectrum      159Ч160
Chloroform, isotope effects      79
Cholestane      215
Cholesteryl acetate, $ ^{13}C$ spectrum      155
Cholesteryl acetate, APT spectrum      155
cis-1,2-Dichlorocyclopropane      104
Cleaning of NMR tubes      33
Closely coupled nuclei      185Ч186 see
Coalescence temperature      142Ч143
Coherence      9 326
Coherence, order      204 326Ч333
Coherence, selection      165 204
Coherence-level diagram      327Ч333
COLOC      192Ч193 264Ч266
Combination line      115 312
Complete line shape analysis      142Ч143
Composite pulses      148Ч165
Conformation      335Ч340
Conformation, anti      335 337Ч339
Conformation, gauche      335 337Ч339
Conformation, population effects      335Ч336 338Ч339
Conjugated coupling      113
Conjugation      see "Resonance effects"
Connectivity      199 203
Contact shifts      321
Continuous-wave operation      7 31 35
Contour Plot      176 250Ч251
Cope rearrangement      140Ч141
COSY      172Ч186 196Ч198 207 208Ч212 217 219 222Ч232 252Ч253 281Ч285 328Ч332
COSY, gradient version      252 see "Phase-sensitive
COSY45      181Ч182 207 211Ч212 252Ч253
Coupling constant      13Ч19 56 98Ч130 302Ч303 305
Coupling constant, mechanism      104Ч105
Coupling constant, relative signs      105
Coupling constant, residual      60Ч61
Coupling constant, sign      104Ч105
Coupling, between equivalent nuclei      98 101 107 118Ч119
Coupling-constant criterion      102 122
Cross peaks      176 330Ч333
Cross polarization      27 185
Cross sections, in spectral analysis      250 see "Contour
Crotonaldehyde, $ ^{1}H$ chemical shift      72
Cubane, $ ^{1}H- ^{13}C$ coupling constant      105
CW      see "Continuous wave"
Cyclobutane, $ ^{13}C$ chemical shift      83
Cyclobutane, $ ^{1}H$ chemical shift      63 69
Cycloheptatriene      124
Cycloheptatrienyltin      142Ч143
Cyclohexane      104
Cyclohexane ring, shielding      66
Cyclohexane, $ ^{13}C$ chemical shift      83
Cyclohexane, dynamic $ ^{1}H$ spectrum      24Ч25
Cyclohexane, HCH coupling      107
Cyclohexane, isotope effects      79
Cyclohexane, ring reversal      137
Cyclohexanes, $ ^{13}C$ chemical shifts      83Ч84 89
Cyclohexanes, long-range coupling      114
Cyclohexanes, vicinal couplings      110
Cyclohexanone $ ^{13}C$ chemical shift      88
Cyclohexene, $ ^{13}C$ chemical shift      86
Cyclohexene, HCCH coupling      112
Cyclooctane, conformation      139
Cyclooctatetraene, bond shifts      141Ч142
Cyclooctatetraene, ring reversal      139
Cyclooctatetreneiron tricarbonyl      142
Cyclopentanol, $ ^{13}C$ chemical shift      85Ч86
Cyclopropane, $ ^{13}C$ chemical shift      83
Cyclopropane, $ ^{1}H$ chemical shift      69
Cyclopropane, $ ^{1}H- ^{13}C$ coupling constant      105
Cyclopropane, HCH coupling      107
Cyclopropane, shielding      67
Cyclopropanes, vicinal couplings      110Ч111
Cyclopropene      100 118Ч119
Cyclopropene, HCCH coupling      112
Cyclops      45 165 180
Dante      166
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