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Cazes J., Scott R.P.W. — Chromatography Theory
Cazes J., Scott R.P.W. — Chromatography Theory

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Название: Chromatography Theory

Авторы: Cazes J., Scott R.P.W.

Аннотация:

This title presents a comprehensive overview of the principles, methods and fundamental theories used in the separation, quantification and analysis of individual compounds and substances. It identifies recent advances, mathematical relationships and useful design techniques for optimal system operation and control of chemical and chromatographic processes.


Язык: en

Рубрика: Химия/

Статус предметного указателя: Готов указатель с номерами страниц

ed2k: ed2k stats

Год издания: 2002

Количество страниц: 475

Добавлена в каталог: 20.04.2006

Операции: Положить на полку | Скопировать ссылку для форума | Скопировать ID
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Предметный указатель
Adlard, E.R.      18
Adsorption isotherm, bi-layer      93 95
Adsorption isotherm, bi-layer, function for      96
Adsorption isotherm, chloroform, butylchloride      94
Adsorption isotherm, effect on peak shape      176
Adsorption isotherm, for alcohols      90
Adsorption isotherm, Freundlich      177
Adsorption isotherm, Langmuir      88
Adsorption isotherm, single layer      88
Alhedai, A.      45
Amundson, N.R.      17
Analysis, quantitative, from retention measurements      171
Arnold, J.H.      359
Ashley, J.W.      233
Asshauer, J.      286
Associated, methanol-water      125
Associated, solvents, solute interactions with      135
Association, methanol-water mixtures, standard enthalpy of      133
Association, methanol-water mixtures, standard entropy of      133
Association, methanol-water, thermodynamic properties      133
Assymetry, peak, causes      175
Atwood, J.G.      286 314
Avaerage mobile phase velocity      272
Available stationary phase      36
Barker, P.E.      442
Base line, definition of      14
Beesley, T.E.      85 142 164
Benedek, P.      442
Bi-layer adsorption      95
Bi-layer adsorption, isotherm for ethyl acetate      97
Bi-layer adsorption, isotherm, function for      96
Bird, R.B.      165
Bonded phase, brush type      92
Bonded phase, bulk type      92
Bonding, stationary phase, effect on retention      92
Bophemen, J.      233
Butyl chloride, adsorption isotherm      94
Capacity, peak, as function of capacity ratio      207
Capacity, peak, equation for      206
Capacity, plate      23
Capacity, ratio, equation for      27
Capacity, ratio, function of temperature      49
Capacity, ratio, limited by detector sensitivity      208
Capacity, ratio, of a solute      26
Cell, detector, low dispersion      308
Chilton, C.H.      234
Chloroform, adsorption isotherm      94
Chromatogram, alternative axes      238
Chromatogram, reduced      362
Chromatography, column design, applications      396
Chromatography, column design, capillary      386
Chromatography, column design, packed      360
Chromatography, column, expression for peak capacity      206
Chromatography, continuous, moving bed      434
Chromatography, continuous, simulated moving bed      439
Chromatography, definition of      4
Chromatography, development      7
Chromatography, preparative      420
Chromatography, terminology      14
Chromatography, theory, history of      4
Chromatography, theory, introduction to      3
Chromatography, thin layer      444
Chromatography, thin layer, effective capacity ratio      450
Chromatography, thin layer, efficiency measurement of      452
Chromatography, thin layer, plate dispersion      453
Chromatography, thin layer, resolution      450
Chromatography, thin layer, Rf factor      448 449
Chromatography, thin layer, Rx factor      448
Chromatography, vacancy      195
Chromatography, vacancy, elution curve equation      197
Chromatography, vacancy, multicomponent mixture      200
Claxton, G.C.      234
Co-elution temperature, expression for      82
Column design, data bases, analytical specifications      367
Column design, data bases, column specifications      366
Column design, data bases, elective variables      365
Column design, data bases, instrument constraints      364
Column design, data bases, performance criteria      362
Column design, optimum particle diameter      371
Column design, process for packed columns      368
Column, capillary, design      386
Column, capillary, maximum sample volume      393
Column, capillary, minimum elution time      392
Column, capillary, minimum H      391
Column, capillary, minimum length      391
Column, capillary, optimum flow rate      392
Column, capillary, optimum radius      389
Column, capillary, optimum velocity      391
Column, dead volume      34
Column, design, applications      396
Column, design, packed column      360
Column, design, protocol      360
Column, dispersion, accurate measurement of      317
Column, efficiency      179
Column, efficiency, expression for      181
Column, efficiency, plates necessary for separation      186
Column, expression for peak capacity      206
Column, moving phase      35
Column, optimized specifications      366
Column, optimized, minimum elution time      376
Column, packed      368
Column, packed, maximum sample volume      384
Column, packed, minimum H      376
Column, packed, minimum length      376
Column, packed, minimum solvent consumption      383
Column, packed, optimum flow rate      382
Column, packed, optimum particle diameter      371
Column, packed, optimum radius      380
Column, packed, optimum velocity      375
Column, packed, sources of dispersion      245
Column, peak capacity      202
Column, permitted extra column volume      290
Column, physical properties of      43
Column, preparative, mass overload      428
Column, preparative, optimum sample size      432
Column, preparative, overload      420
Column, preparative, volume overload      421
Column, resolving power      183
Column, static phase      35
Column, volume, distribution of      35
Compressibility , mobile phase      28
Conduits, tubular, dispersion in      296
Continuous chromatography, moving bed      434
Curtis, C.F.      164
Davis, J.M.      234
Dead, point, definition of      14
Dead, time, definition of      15
Dead, volume, definition of      15
Dead, volume, measurement of      39
Deeble, R.E.      442
Density, change on mixing, methanol-water      128
Design protocol, column      360
Desty, D.H.      233
Detector cell low dispersion      308
Detector, heat of adsorption, theory of      218
Detector, sensor volume, apparent dispersion      307
Detector, sensor volume, dispersion from Newtonian flow      306
Development, chromatographic      7
Development, displacement      7
Development, elution      9
Development, elution in TLC      12
Development, frontal analysis      8
Development, solvent profile in TLC      13
Diffusion, dispersion equation      245
Diffusion, eddy      246
Diffusion, effect of column pressure      275
Diffusion, effect of pressure on dispersion in LC      276
Diffusion, Ficks law      243
Diffusion, liquid, effect of pressure      274
Diffusion, process      243
Diffusivity, function of molecular weight      339
Dipole moment, effect on dipole interactions      66
Dipole-dipole interactions      66
Dipole-induced-dipole interactions      67
dispersion      317
Dispersion, detector sensor volume apparant      307
Dispersion, detector sensor volume apparant, Newtonian flow      306
Dispersion, dynamics of      237
Dispersion, effect of detector time constant      311
Dispersion, extra column      288
Dispersion, extra column, maximum for a capillary column      393
Dispersion, extra column, sources      291
Dispersion, forces, effect of polarizability      64
Dispersion, forces, interaction energy of      64
Dispersion, from Newtonian flow      297
Dispersion, from sample volume      291
Dispersion, in a packed bed      245
Dispersion, in frits      295
Dispersion, in sample valves      294
Dispersion, in tubular conduits      296
Dispersion, in unions      295
Dispersion, interactive force      63
Dispersion, longitudinal diffusion      248
Dispersion, longitudinal diffusion, expression for mobile phase      249
Dispersion, longitudinal diffusion, expression for stationary phase      250
Dispersion, low, connecting tube      301
Dispersion, low, serpentine tubes      303
Dispersion, mobile phase, HETP equation corrected for gas compressibility      271
Dispersion, multipath, effect      246
Dispersion, multipath, expression for      247
Dispersion, on a thin layer plate      453
Dispersion, packed column, mobile phase compressibility effect on HETP      268
Dispersion, packed column, relationship to molecular weight      344
Dispersion, radial      240
Dispersion, radial, expression for      242
Dispersion, resistance to mass transfer, mobile phase      251
Dispersion, resistance to mass transfer, stationary phase      252
Dispersion, resistance to mass transfer, stationary phase expression      256
Displacement, development      7
Distribution coefficient, effect of temperature      49
Distribution coefficient, function of free energy      47
Distribution coefficient, in plate equilibrium      21
Distribution coefficient, retention control      47
Distribution coefficient, thermodynamic treatment      47
Done, J.N.      286
Dreyer, B.      45
Dynamics of peak dispersion      237
D’Arcy's equation      29
Eddy diffusion      246
Effective plate number      187
Effective plate number, equation for      188
Effective plate number, relationship to efficiency      189 190
Efficiency, column      179
Efficiency, column, expression for      181
Efficiency, column, plates necessary for resolution      186
Efficiency, relationship to effective plate number      189
Elective variables      365
Electron acceptor sites      76
Electron doner sites      76
Elution, curve, equation for      23
Elution, development in TLC      12
Elution, equation, Gaussian form      165
Elution, of a finite sample      190
Elution, of a finite sample, expression for      192
Elution, process of      9
Enantiomeric separations      81
Endele, R.      286
Energy driven distribution      50
Engelhardt, H.      45
Enthalpy, control of distribution      50
Enthalpy, from Vant Hoff curves      49
Enthalpy, physical significance      48
Enthalpy, positive effect on distribution      53
Enthalpy, standard, free      48
Enthalpy, standard, relationship with standard entropy      61
Entropy driven distribution      51
Entropy, control of distribution      50
Entropy, from Vant Hoff curves      49
Entropy, negative effect on distribution      53
Entropy, physical significance      48
Entropy, standard, for different group types      58
Entropy, standard, free      48
Entropy, standard, relationship with standard enthalpy      61
Eon, C.      313
Equilibrium, established between phases      11
Equilibrium, in a theoretical plate      21
Exit velocity, mobile phase      273
Extensions of the HETP equation      277
Extra column dispersion      288
Extra column dispersion, permitted for different columns      290
Extra column dispersion, sources of      291
Extra column volume      25
Eyring, H.      359
Feller, W.      260
Ficks law      244
Flow, optimum for capillary column      392
Flow, optimum for maximized column      382
Flow, programming      144
Flow, programming, compressible fluid, GC      146
Flow, programming, effect on retention time GC      149
Flow, programming, non compressible fluid, LC      144
Free energy, control of distribution      47
Free energy, distribution between groups      57
Free energy, distribution between interaction types      75
Free energy, standard      48
Freund, M.      442
Freundlich adsorption isotherm      177
Frits, dispersion in      295
Frontal analysis      8
Fudge factors      258
Geiss, F.      455
Gerlach, H.O.      313
Giddings equation      262
Giddings, J.C.      18 233 234 260 285 286 419 455
Gilbert, M.T.      313
Glasstone, S.      85
Gluekauf, E.      17
Golay equation      267
Golay, M.J.E.      18 45 261 286 314
Goldstein, J.      286
Goldup, A.      233
Golshan-Shirazi, S.      18 442
Gradient elution      157
Groszek, A.J.      234
Grushka, E.      359
Guiochon, G.      18 313 442
Gutierrez, J.E.N.      142
Gutlich, K.F.      313
Halasz, L.      286 313
Heat of adsorption detector, theory of      218
Height, of a theoretical plate      239
Height, peak, definition of      16
Height, peak, measurement, effect of assymetry      170
Herington, E.F.G.      18
HETP, minimum      279
Hildebrand, C.P.      233
Hirschfelder, J.O.      164
History of chromatography theory      4
Hofmann      313
Homologous series, thermodynamic analysis of      54
Horne, D.S.      260
Horvath and Lin equation      266
Horvath, Cs.      18 286 455
Huber equation      263
Huber, J.F.K.      18 285 286
Hulsman, A.R.J.      18 285
Hurrel, R.      442
Hurtubise, R.J.      142
Hussain, A.      142
Hydrophilic interactions      71
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