The Laboratory Manual is intended to accompany the Textbook to permit teaching radioanalytical chemistry to seniors and graduate students in a program that will train radiochemists, who are badly needed at this time. The manual will be used in conjunction with the textbook to teach a 3–hour lecture course and a 6–hour laboratory. The experiments address a range of practical aspects in the radiochemistry laboratory: use of laboratory and radiation detection equipment, performing specific analyses for radio–iodine, radio–strontium, uranium, and plutonium, and developing the skill of selecting and testing new procedures.