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Armarego W.L.F., Li Lin Chai C. — Purification of Laboratory Chemicals
Armarego W.L.F., Li Lin Chai C. — Purification of Laboratory Chemicals



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Название: Purification of Laboratory Chemicals

Авторы: Armarego W.L.F., Li Lin Chai C.

Аннотация:

This monograph remains the bible for practising chemists wishing to know how to dry solvents or purify commercially available laboratory chemicals...The authors have made good use of computerised databases for up to date information and have placed a noticeable emphasis on safety. It is of manageable size and, like its forebears, will be the most commonly used reference book in any chemical or biochemical laboratory.


Язык: en

Рубрика: Химия/

Статус предметного указателя: Готов указатель с номерами страниц

ed2k: ed2k stats

Издание: 5-th

Год издания: 2003

Количество страниц: 608

Добавлена в каталог: 10.10.2006

Операции: Положить на полку | Скопировать ссылку для форума | Скопировать ID
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Предметный указатель
$\mathrm{BH_42HC1}$      514
$\mathrm{DTBC1}_2$      382
2, 4-D      177
2, 4-DP      177
3'-AMP      461
5'-AMP      461
5-HT      511
9 BBN      370
Abderhalden pistol      15
Aces      64
Acetals, drying agent for      38
Acetals, drying agent for, purification of      54
AcetamidoTEMPO      65
Acid anhydrides, purification of      56
Acid chlorides, purification of      55
Acids, drying agents for      38
Acids, drying agents for, purification of      55
Acyl halides, drying agents for      38
Ada      65
ADP      461
Adsorbents, for chromatography      18 19 38
Aerosol-OT      426
AICARHC1      88
Alcohols, drying agents for      38
Alcohols, drying agents for, purification of      55 56
Alcohols, drying agents for, purification via derivatives.      50
Aldehydes, drying agents for      38
Aldehydes, drying agents for, purification of      56
Aldehydes, drying agents for, purification using ion-exchange      21
Aldehydes, drying agents for, purification via derivatives.      51
Aliphatic acids, purification of      52 55
Aliphatic halides, purification of      58
Alkyl halides, drying agents for      38
Alumina      18
Alumina as drying agent      16
Alumina for chromatography      18
Alumina, activation of      18
Alumina, grades of      19
Alumina, preparation of neutral      19
Aluminium amalgam, as drying agent      16 209 260
Aluminium amalgam, as drying agent, preparation of      209 260
Aluminium methoxide, preparation of      260
Amberlite IRA-400, preparation of OH-form      336
Amechol      459
Amides, purification of      56
Amines, drying agents for      38
Amines, drying agents for, purification as double salts.      51
Amines, drying agents for, purification as N-acetyl derivatives      51
Amines, drying agents for, purification as N-tosyl derivatives      52
Amines, drying agents for, purification as picrates      51
Amines, drying agents for, purification as salts      51
Amines, drying agents for, purification of      56
Amino acids, purification of      56
Amino acids, purification of, purification by ion-exchange      21
Aminosugars, purification by ion-exchange      21
Analytical ultracentrifuge      454
Anhydrides, purification of      56
Apparatus, cleaning      4
Aromatic hydrocarbons, purification via derivatives      52
Aryl halides, drying agents for      38
Ascarite      366
Atroscine      243
Azeotropic mixtures      11
Azeotropic mixtures, separation of      11
Barium oxide, as drying agent      16
Barium perchlorate, as drying agent      16
Basic Red      5 283
BBOD      467
Benzethionium chloride      235
BES      114
BHT      172
Bial’s orcinol reagent      460
Bis-Tris      114
BMS      467
Boiling point, variation with pressure      5 6 31 32
Boric anhydride, as drying agent      16
Boric anhydride, as drying agent, preparation of      16
Bruun column      8
Bubble-cap column      8
Buckminster fullerene      224
Buckyball      224
Buffer solutions      43
Bumping, prevention in distillation      7
Calcium chloride, as drying agent      16
Calcium hydride      49
Calcium oxide, as drying agent      16
Calcium sulphate, as drying agent      16
Calcymycin      374
Capillary electrophoresis      455
Carbic anhydride      289
Carboxylic acids, purification of      55
Carboxylic acids, purification of, purification via derivatives      52
Carotenoids, purification of      57
Catapres      472
Catharometer      25
Cation exchange resins      470
CDTA      158
Celite, purification of      19
Cellex CM      22
Cellex D      22
Cellulose, for chromatography      19
Centrifugation      454
Centrifugation in purification      13
Charcoal, activation of      19
Charcoal, activation of, decolorising with      12
Charcoal, activation of, purification of      138
Chelex      22 39 48 455
Chemical hazards      29 30
Chromatofocusing      455
Chromatography      18
Chromatography, adsorbents for      18 38
Chromatography, adsorption      18
Chromatography, affinity      24 455 457
Chromatography, charge-transfer adsorption      23
Chromatography, columns for HPLC      40 41
Chromatography, covalent      24
Chromatography, flash      20
Chromatography, gas      24 (see also “Vapour phase”)
Chromatography, high performance liquid      23 40 41
Chromatography, hydrophobic adsorption      24
Chromatography, ion-exchange      21
Chromatography, metal-chelate adsorption      24
Chromatography, paired-ion      20
Chromatography, paper      26
Chromatography, partition      20
Chromatography, solvents for      38
Chromatography, standardisation of alumina      18
Chromatography, thin or thick layer      26
Chromatography, vapour phase      24
Chromatotron      27
Chromic acid, cleaning mixture      4 12
Citiolone      72
Citronin A      281
Claisen alkali      379
Claisen flask      7
Cleland’s reagent      204
Condensers      8 9
Condensers, air      8
Condensers, Allihn      9
Condensers, Allihn — Kronbitter      9
Condensers, Bailey — Walker      9
Condensers, coil      9
Condensers, double-surface      9
Condensers, Friedrichs      9
Condensers, Graham      9
Condensers, Hopkins      9
Condensers, Julian      9
Condensers, Liebig      9
Condensers, Othmer      9
Condensers, West      9
Condensers, Wiley      9
Cooling baths      36
Copper sulphate, as drying agent      16
Copper-zinc couple      216
Cosbiol      512
Counter-current distribution      28
Cryostats      36
CTAB      233
Cytovene      486
D-quinovose      165
Dag      186
DATD      166
Davy’s reagent      369
DBN      169
DDQ      175
DDT      113
dead      180
Dehydrite      17
DEP      182
Desiccants      16-17
Dextrans      22 23
DHFA      479
Dialysis      456
Diatomaceous earth      376
Diatomaceous earth for chromatography      19
Diazald      272
DIPHOS      214
Disperse Blue      114
Distillation      5 48
Distillation at atmospheric pressure      7
Distillation columns      7 8
Distillation columns, Bruun      8
Distillation columns, bubble-cap      8
Distillation columns, Dufton      8
Distillation columns, Hempel      8
Distillation columns, Oldershaw      8
Distillation columns, Podbielniak      8
Distillation columns, Stedman      8
Distillation columns, Todd      8
Distillation columns, Vigreux      8
Distillation columns, Widmer      8
Distillation, azeotropic      11
Distillation, bumping, prevention of      7
Distillation, efficiency      6 7
Distillation, fractional      6
Distillation, isopiestic      11
Distillation, isothermal      11 48
Distillation, kugelrohr      10
Distillation, steam      10
Distillation, techniques      6
Distillation, vacuum      9
Distribution, between solvents      27
Disulphides, purification of      60
Disulphoxides, purification of      60
Diuron      177
Dixon rings      8
DMF      192
DMSO      196
DMT      188
DNA, purification of      457
DNA, purification of, concentration      457 458
DNA, purification of, determination of      458
DOPA      480
DPN      498
Drierite      16
Drying      15
Drying agents      16 38
Drying pistol      15
Drying pistol, liquids for      37
DTE      204
Dufton column      8
EDTA      214
EGTA      215
Ehrlich’s Reagent      189
Emulsions, breaking of      28
Esculetin      185
Esters, drying agents for      38
Esters, drying agents for, purification of      57
ETH 1001      374
ETH 1117      400
ETH 129      374
ETH 149      383
ETH 1778      393
ETH 1907      393
ETH 227      430
ETH 4120      430
ETH 5214      400
ETH 5294      378
ETH 6010      375
Ethanol, azeotropic drying      11
Ethers, drying agents for      38
Ethers, drying agents for, purification of      57
Euflavin      76
EUODOPA      480
FAD      484
Fast Garnet GBC base      85
Fenske rings      8
Fieser’s solution      406
Filter paper, properties of      33 34
Filter paper, properties of, for removal of trace metals      19
Filters      34
Filters, membranes      34
Filters, millipore      34
Filters, nucleopore      34
Filters, Sartorius membrane      34
Filtration      13
Flophemesyl chloride      408
FMN      484
FMOC-C1      221
Folliculin      208
Footballene      224
Formaldehyde from paraldehyde      222
Fractional solidification      14
Fractogels      22 40 455
Freeze-pump-thaw degassing      17
Freon      122
FSH      485
Gas chromatography      see “Vapour phase”
Gas chromatography, chromatography      24
Gases, boiling points      37
GDH      487
Gel electrophoresis      456 457
Gel filtration      23 27 454
Gentian violet      154
Glovebox techniques      10
Glyme      188
Heating baths      33
Heimgartner’s reagent      370
Hempel column      8
HEPES      238
Heterocyclic bases, drying agents for      38
HETP      6
Hexadimethrene      192
HMPT      391
HPLC      23 455 457
Hydrocarbons, drying agents for      38
Hydrocarbons, drying agents for, purification of      58
Hydrochloric acid, constant boiling      392
Hydroperoxides, purification via derivatives      52
Hydroxy lapatite      22 455
Imides, purification of      59
Imino compounds, purification of      59
Ion-exchange celluloses      21 22
Ion-exchange chromatography      21
Ion-exchange resins      21 39 48 455
Ion-exchange resins, affinity for ions      21
Ion-exchange resins, bead form      40
Ion-exchange resins, preparation of columns      22
Iron, removal by precipitation      49
Isoelectric focusing      455
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